Study of adhesive bondlines in modified wood with fluorescence microscopy and X-ray micro-computed tomography.

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Title: Study of adhesive bondlines in modified wood with fluorescence microscopy and X-ray micro-computed tomography.
Authors: Bastani, Alireza1 abastan@gwdg.de, Adamopoulos, Stergios2, Koddenberg, Tim1, Militz, Holger1
Source: International Journal of Adhesion & Adhesives. Jul2016, Vol. 68, p351-358. 8p.
Subjects: Adhesive joints, Fluorescence microscopy, X-ray computed microtomography, Wood, Emulsion polymerization, Heat treatment
Abstract: The quantitative penetration of three coldset wood adhesives [one-component polyurethane (PU), emulsion polymer isocyanate (EPI), poly (vinyl acetate) (PVAc)] under hydraulic pressure into different types of modified wood was studied using fluorescence microscopy and the results were compared to these of a previous study without pressure on adjacent wood samples. The effective penetration (EP) of PU was negatively affected by furfurlylation and NMM modification when pressure was applied. For PVAc, 30% NMM treatment and heat treatment of Scots pine and beech at 210 °C had a negative effect on its EP, but against this the EP of this adhesive increased after heat treatment of beech at 195 °C. In the case of furfurylation, the depth of penetration of all adhesives was less into wood treated with higher concentration of furfuryl alcohol. PU showed a much deeper penetration into NMM-modified and heat-treated wood than the other adhesives with the exception of heat-treated beech at 195 °C. Application of pressure led to rather different results as compared to the EP data when no pressure was applied. The three-dimensional (3D) visualisation of the penetration of PU adhesive into heat-treated Scots pine was also examined by X-ray micro-computed tomography (XµCT). The 3D flow pattern of PU adhesive into heat-treated Scots pine was clearly depicted by XµCT. [ABSTRACT FROM AUTHOR]
Copyright of International Journal of Adhesion & Adhesives is the property of Elsevier B.V. and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)
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  Data: Study of adhesive bondlines in modified wood with fluorescence microscopy and X-ray micro-computed tomography.
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  Data: <searchLink fieldCode="AR" term="%22Bastani%2C+Alireza%22">Bastani, Alireza</searchLink><relatesTo>1</relatesTo><i> abastan@gwdg.de</i><br /><searchLink fieldCode="AR" term="%22Adamopoulos%2C+Stergios%22">Adamopoulos, Stergios</searchLink><relatesTo>2</relatesTo><br /><searchLink fieldCode="AR" term="%22Koddenberg%2C+Tim%22">Koddenberg, Tim</searchLink><relatesTo>1</relatesTo><br /><searchLink fieldCode="AR" term="%22Militz%2C+Holger%22">Militz, Holger</searchLink><relatesTo>1</relatesTo>
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  Data: <searchLink fieldCode="JN" term="%22International+Journal+of+Adhesion+%26+Adhesives%22">International Journal of Adhesion & Adhesives</searchLink>. Jul2016, Vol. 68, p351-358. 8p.
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  Data: <searchLink fieldCode="DE" term="%22Adhesive+joints%22">Adhesive joints</searchLink><br /><searchLink fieldCode="DE" term="%22Fluorescence+microscopy%22">Fluorescence microscopy</searchLink><br /><searchLink fieldCode="DE" term="%22X-ray+computed+microtomography%22">X-ray computed microtomography</searchLink><br /><searchLink fieldCode="DE" term="%22Wood%22">Wood</searchLink><br /><searchLink fieldCode="DE" term="%22Emulsion+polymerization%22">Emulsion polymerization</searchLink><br /><searchLink fieldCode="DE" term="%22Heat+treatment%22">Heat treatment</searchLink>
– Name: Abstract
  Label: Abstract
  Group: Ab
  Data: The quantitative penetration of three coldset wood adhesives [one-component polyurethane (PU), emulsion polymer isocyanate (EPI), poly (vinyl acetate) (PVAc)] under hydraulic pressure into different types of modified wood was studied using fluorescence microscopy and the results were compared to these of a previous study without pressure on adjacent wood samples. The effective penetration (EP) of PU was negatively affected by furfurlylation and NMM modification when pressure was applied. For PVAc, 30% NMM treatment and heat treatment of Scots pine and beech at 210 °C had a negative effect on its EP, but against this the EP of this adhesive increased after heat treatment of beech at 195 °C. In the case of furfurylation, the depth of penetration of all adhesives was less into wood treated with higher concentration of furfuryl alcohol. PU showed a much deeper penetration into NMM-modified and heat-treated wood than the other adhesives with the exception of heat-treated beech at 195 °C. Application of pressure led to rather different results as compared to the EP data when no pressure was applied. The three-dimensional (3D) visualisation of the penetration of PU adhesive into heat-treated Scots pine was also examined by X-ray micro-computed tomography (XµCT). The 3D flow pattern of PU adhesive into heat-treated Scots pine was clearly depicted by XµCT. [ABSTRACT FROM AUTHOR]
– Name: AbstractSuppliedCopyright
  Label:
  Group: Ab
  Data: <i>Copyright of International Journal of Adhesion & Adhesives is the property of Elsevier B.V. and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.)
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RecordInfo BibRecord:
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      – Type: doi
        Value: 10.1016/j.ijadhadh.2016.04.006
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      – Code: eng
        Text: English
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        PageCount: 8
        StartPage: 351
    Subjects:
      – SubjectFull: Adhesive joints
        Type: general
      – SubjectFull: Fluorescence microscopy
        Type: general
      – SubjectFull: X-ray computed microtomography
        Type: general
      – SubjectFull: Wood
        Type: general
      – SubjectFull: Emulsion polymerization
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      – SubjectFull: Heat treatment
        Type: general
    Titles:
      – TitleFull: Study of adhesive bondlines in modified wood with fluorescence microscopy and X-ray micro-computed tomography.
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            NameFull: Bastani, Alireza
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            NameFull: Adamopoulos, Stergios
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            NameFull: Koddenberg, Tim
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            NameFull: Militz, Holger
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            – D: 01
              M: 07
              Text: Jul2016
              Type: published
              Y: 2016
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              Value: 68
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            – TitleFull: International Journal of Adhesion & Adhesives
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