Synthesis and magnetic properties of cobalt ferrite nanoparticles in polycarbosilane ceramic matrix.

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Title: Synthesis and magnetic properties of cobalt ferrite nanoparticles in polycarbosilane ceramic matrix.
Authors: Yurkov, Gleb Yu.1, Shashkeev, Konstantin A.2 shashkon@yandex.ru, Kondrashov, Stanislav V.2, Popkov, Oleg. V.2, Shcherbakova, Galina I.3, Zhigalov, Dmitrii V.3, Pankratov, Denis A.4, Ovchenkov, Evgeny A.5, Koksharov, Yury A.5,6
Source: Journal of Alloys & Compounds. Nov2016, Vol. 686, p421-430. 10p.
Subjects: Magnetic properties of transition metal compounds, Cobalt compounds, Nanoparticle synthesis, Polysilanes, Ceramic metals, Chemical sample preparation, Sintering
Abstract: Composite materials comprised of a ceramic matrix with metal-containing nanoparticles were prepared by sintering a blend of cobalt ferrite nanoparticles and polycarbosilane. Sintering process was performed either in air or argon, resulting in different material composition. The air-sintering materials consist mainly of oxide phases (silica matrix and cobalt ferrite nanoparticles). The process of sintering in argon leads to partial reduction of oxides and formation of α-Fe, carbide and silicate phases. The prepared samples were characterized by the SEM, TEM, XRD and EMR techniques and the Mössbauer spectroscopy. Static magnetic properties were also studied. All samples were found to be soft magnetic. Sintering, especially in argon, increases remnant magnetization of resulting composite products. [ABSTRACT FROM AUTHOR]
Copyright of Journal of Alloys & Compounds is the property of Elsevier B.V. and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)
Database: Engineering Source
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Header DbId: egs
DbLabel: Engineering Source
An: 117733989
AccessLevel: 6
PubType: Academic Journal
PubTypeId: academicJournal
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  Data: Synthesis and magnetic properties of cobalt ferrite nanoparticles in polycarbosilane ceramic matrix.
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  Data: <searchLink fieldCode="AR" term="%22Yurkov%2C+Gleb+Yu%2E%22">Yurkov, Gleb Yu.</searchLink><relatesTo>1</relatesTo><br /><searchLink fieldCode="AR" term="%22Shashkeev%2C+Konstantin+A%2E%22">Shashkeev, Konstantin A.</searchLink><relatesTo>2</relatesTo><i> shashkon@yandex.ru</i><br /><searchLink fieldCode="AR" term="%22Kondrashov%2C+Stanislav+V%2E%22">Kondrashov, Stanislav V.</searchLink><relatesTo>2</relatesTo><br /><searchLink fieldCode="AR" term="%22Popkov%2C+Oleg%2E+V%2E%22">Popkov, Oleg. V.</searchLink><relatesTo>2</relatesTo><br /><searchLink fieldCode="AR" term="%22Shcherbakova%2C+Galina+I%2E%22">Shcherbakova, Galina I.</searchLink><relatesTo>3</relatesTo><br /><searchLink fieldCode="AR" term="%22Zhigalov%2C+Dmitrii+V%2E%22">Zhigalov, Dmitrii V.</searchLink><relatesTo>3</relatesTo><br /><searchLink fieldCode="AR" term="%22Pankratov%2C+Denis+A%2E%22">Pankratov, Denis A.</searchLink><relatesTo>4</relatesTo><br /><searchLink fieldCode="AR" term="%22Ovchenkov%2C+Evgeny+A%2E%22">Ovchenkov, Evgeny A.</searchLink><relatesTo>5</relatesTo><br /><searchLink fieldCode="AR" term="%22Koksharov%2C+Yury+A%2E%22">Koksharov, Yury A.</searchLink><relatesTo>5,6</relatesTo>
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  Data: <searchLink fieldCode="JN" term="%22Journal+of+Alloys+%26+Compounds%22">Journal of Alloys & Compounds</searchLink>. Nov2016, Vol. 686, p421-430. 10p.
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  Data: <searchLink fieldCode="DE" term="%22Magnetic+properties+of+transition+metal+compounds%22">Magnetic properties of transition metal compounds</searchLink><br /><searchLink fieldCode="DE" term="%22Cobalt+compounds%22">Cobalt compounds</searchLink><br /><searchLink fieldCode="DE" term="%22Nanoparticle+synthesis%22">Nanoparticle synthesis</searchLink><br /><searchLink fieldCode="DE" term="%22Polysilanes%22">Polysilanes</searchLink><br /><searchLink fieldCode="DE" term="%22Ceramic+metals%22">Ceramic metals</searchLink><br /><searchLink fieldCode="DE" term="%22Chemical+sample+preparation%22">Chemical sample preparation</searchLink><br /><searchLink fieldCode="DE" term="%22Sintering%22">Sintering</searchLink>
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  Data: Composite materials comprised of a ceramic matrix with metal-containing nanoparticles were prepared by sintering a blend of cobalt ferrite nanoparticles and polycarbosilane. Sintering process was performed either in air or argon, resulting in different material composition. The air-sintering materials consist mainly of oxide phases (silica matrix and cobalt ferrite nanoparticles). The process of sintering in argon leads to partial reduction of oxides and formation of α-Fe, carbide and silicate phases. The prepared samples were characterized by the SEM, TEM, XRD and EMR techniques and the Mössbauer spectroscopy. Static magnetic properties were also studied. All samples were found to be soft magnetic. Sintering, especially in argon, increases remnant magnetization of resulting composite products. [ABSTRACT FROM AUTHOR]
– Name: AbstractSuppliedCopyright
  Label:
  Group: Ab
  Data: <i>Copyright of Journal of Alloys & Compounds is the property of Elsevier B.V. and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.)
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RecordInfo BibRecord:
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      – Type: doi
        Value: 10.1016/j.jallcom.2016.06.025
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      – Code: eng
        Text: English
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        PageCount: 10
        StartPage: 421
    Subjects:
      – SubjectFull: Magnetic properties of transition metal compounds
        Type: general
      – SubjectFull: Cobalt compounds
        Type: general
      – SubjectFull: Nanoparticle synthesis
        Type: general
      – SubjectFull: Polysilanes
        Type: general
      – SubjectFull: Ceramic metals
        Type: general
      – SubjectFull: Chemical sample preparation
        Type: general
      – SubjectFull: Sintering
        Type: general
    Titles:
      – TitleFull: Synthesis and magnetic properties of cobalt ferrite nanoparticles in polycarbosilane ceramic matrix.
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            NameFull: Yurkov, Gleb Yu.
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            NameFull: Kondrashov, Stanislav V.
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            NameFull: Popkov, Oleg. V.
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              Text: Nov2016
              Type: published
              Y: 2016
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