A Simple Vortex-Assisted Dispersive Liquid-Liquid Microextraction System for Copper(II) to Preconcentration and Separation from Natural Water and Table Salt Samples.

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Title: A Simple Vortex-Assisted Dispersive Liquid-Liquid Microextraction System for Copper(II) to Preconcentration and Separation from Natural Water and Table Salt Samples.
Authors: Soylak, M.1 soylak@erciyes.edu.tr, Kiranartligiller, E.1
Source: Arabian Journal for Science & Engineering (Springer Science & Business Media B.V. ). Jan2017, Vol. 42 Issue 1, p175-181. 7p.
Subjects: Copper content of water, Salt analysis, Water sampling, Liquid-liquid extraction, Chemical preconcentration
Abstract: A simple and novel vortex-assisted dispersive liquid-liquid microextraction method for the preconcentration and separation of copper(II) as 1-(2-pyridylazo)-2-naphthol chelates has been presented. 1-decanol and ethanol were used as the extraction solvent and as the dispersive solvent, respectively. The analytical parameters including pH, amount of 1-(2-pyridylazo)-2-naphthol, volume of 1-decanol, volume of ethanol, sample volume which were affected extraction efficiency of copper(II) were optimized. The effects of some matrix components were investigated. The detection limit for copper(II) was $${6.6\, {\rm \mu{g}\,{L}}^{-1}}$$ . The preconcentration factor of method was calculated as 30. The method was validated by the analysis of water certified references materials. The application of the method was done for determination of copper levels of water and table salt samples. [ABSTRACT FROM AUTHOR]
Copyright of Arabian Journal for Science & Engineering (Springer Science & Business Media B.V. ) is the property of Springer Nature and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)
Database: Engineering Source
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  Data: <searchLink fieldCode="DE" term="%22Copper+content+of+water%22">Copper content of water</searchLink><br /><searchLink fieldCode="DE" term="%22Salt+analysis%22">Salt analysis</searchLink><br /><searchLink fieldCode="DE" term="%22Water+sampling%22">Water sampling</searchLink><br /><searchLink fieldCode="DE" term="%22Liquid-liquid+extraction%22">Liquid-liquid extraction</searchLink><br /><searchLink fieldCode="DE" term="%22Chemical+preconcentration%22">Chemical preconcentration</searchLink>
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  Data: A simple and novel vortex-assisted dispersive liquid-liquid microextraction method for the preconcentration and separation of copper(II) as 1-(2-pyridylazo)-2-naphthol chelates has been presented. 1-decanol and ethanol were used as the extraction solvent and as the dispersive solvent, respectively. The analytical parameters including pH, amount of 1-(2-pyridylazo)-2-naphthol, volume of 1-decanol, volume of ethanol, sample volume which were affected extraction efficiency of copper(II) were optimized. The effects of some matrix components were investigated. The detection limit for copper(II) was $${6.6\, {\rm \mu{g}\,{L}}^{-1}}$$ . The preconcentration factor of method was calculated as 30. The method was validated by the analysis of water certified references materials. The application of the method was done for determination of copper levels of water and table salt samples. [ABSTRACT FROM AUTHOR]
– Name: AbstractSuppliedCopyright
  Label:
  Group: Ab
  Data: <i>Copyright of Arabian Journal for Science & Engineering (Springer Science & Business Media B.V. ) is the property of Springer Nature and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.)
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        Value: 10.1007/s13369-016-2208-1
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      – Code: eng
        Text: English
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        PageCount: 7
        StartPage: 175
    Subjects:
      – SubjectFull: Copper content of water
        Type: general
      – SubjectFull: Salt analysis
        Type: general
      – SubjectFull: Water sampling
        Type: general
      – SubjectFull: Liquid-liquid extraction
        Type: general
      – SubjectFull: Chemical preconcentration
        Type: general
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      – TitleFull: A Simple Vortex-Assisted Dispersive Liquid-Liquid Microextraction System for Copper(II) to Preconcentration and Separation from Natural Water and Table Salt Samples.
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              Text: Jan2017
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              Y: 2017
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