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Synthesis of BaFe1‐xNixCuxO3‐δ new ceramic composition as solid oxide fuel cell cathode by microwave‐assisted solid‐state reaction.

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Title: Synthesis of BaFe1‐xNixCuxO3‐δ new ceramic composition as solid oxide fuel cell cathode by microwave‐assisted solid‐state reaction.
Authors: Moghaddas, Shahab1 s17.moghadas@gmail.com, Maghsoudipour, Amir1, Ebadzadeh, Touradj1
Source: Asia-Pacific Journal of Chemical Engineering. Jul2018, Vol. 13 Issue 4, p1-1. 11p.
Subjects: Solid oxide fuel cells, Microwaves, Iron ions, Scanning electron microscopy, X-ray diffraction
Abstract: Abstract: In this research, new ceramic BaFe0.8Ni0.1Cu0.1O3‐δ powder was synthesized by solid‐state reaction method in conventional and microwave furnaces. Then, characterization, structure, and morphology of the resulting powders were studied. For characterization of synthetic powders, X‐ray diffraction, powder density gas pycnometer method, particle size analysis, scanning electron microscopy, and energy‐dispersive spectroscopy were performed. The results showed that the BaFe0.8Ni0.1Cu0.1O3‐δ powder synthesized in microwave furnace at 1,000 °C without soaking time and in conventional furnace at the same temperature with 12‐hr soaking time. In addition, the X‐ray diffraction results demonstrated that the main peak is shifted to lower angles by substitution iron ions with nickel and copper ions. Furthermore, the crystal structures of powders were hexagonal and tetragonal, and their density were 5.88 and 5.43 g/cm3, respectively, in conventional and microwave furnaces. Finally, the morphology and particle size of the synthesized powders were the same in both furnaces. [ABSTRACT FROM AUTHOR]
Copyright of Asia-Pacific Journal of Chemical Engineering is the property of Wiley-Blackwell and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)
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  Data: Synthesis of BaFe<subscript>1‐x</subscript>Ni<subscript>x</subscript>Cu<subscript>x</subscript>O<subscript>3‐δ</subscript> new ceramic composition as solid oxide fuel cell cathode by microwave‐assisted solid‐state reaction.
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  Data: <searchLink fieldCode="AR" term="%22Moghaddas%2C+Shahab%22">Moghaddas, Shahab</searchLink><relatesTo>1</relatesTo><i> s17.moghadas@gmail.com</i><br /><searchLink fieldCode="AR" term="%22Maghsoudipour%2C+Amir%22">Maghsoudipour, Amir</searchLink><relatesTo>1</relatesTo><br /><searchLink fieldCode="AR" term="%22Ebadzadeh%2C+Touradj%22">Ebadzadeh, Touradj</searchLink><relatesTo>1</relatesTo>
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  Data: <searchLink fieldCode="JN" term="%22Asia-Pacific+Journal+of+Chemical+Engineering%22">Asia-Pacific Journal of Chemical Engineering</searchLink>. Jul2018, Vol. 13 Issue 4, p1-1. 11p.
– Name: Subject
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  Data: <searchLink fieldCode="DE" term="%22Solid+oxide+fuel+cells%22">Solid oxide fuel cells</searchLink><br /><searchLink fieldCode="DE" term="%22Microwaves%22">Microwaves</searchLink><br /><searchLink fieldCode="DE" term="%22Iron+ions%22">Iron ions</searchLink><br /><searchLink fieldCode="DE" term="%22Scanning+electron+microscopy%22">Scanning electron microscopy</searchLink><br /><searchLink fieldCode="DE" term="%22X-ray+diffraction%22">X-ray diffraction</searchLink>
– Name: Abstract
  Label: Abstract
  Group: Ab
  Data: Abstract: In this research, new ceramic BaFe0.8Ni0.1Cu0.1O3‐δ powder was synthesized by solid‐state reaction method in conventional and microwave furnaces. Then, characterization, structure, and morphology of the resulting powders were studied. For characterization of synthetic powders, X‐ray diffraction, powder density gas pycnometer method, particle size analysis, scanning electron microscopy, and energy‐dispersive spectroscopy were performed. The results showed that the BaFe0.8Ni0.1Cu0.1O3‐δ powder synthesized in microwave furnace at 1,000 °C without soaking time and in conventional furnace at the same temperature with 12‐hr soaking time. In addition, the X‐ray diffraction results demonstrated that the main peak is shifted to lower angles by substitution iron ions with nickel and copper ions. Furthermore, the crystal structures of powders were hexagonal and tetragonal, and their density were 5.88 and 5.43 g/cm3, respectively, in conventional and microwave furnaces. Finally, the morphology and particle size of the synthesized powders were the same in both furnaces. [ABSTRACT FROM AUTHOR]
– Name: AbstractSuppliedCopyright
  Label:
  Group: Ab
  Data: <i>Copyright of Asia-Pacific Journal of Chemical Engineering is the property of Wiley-Blackwell and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.)
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    Identifiers:
      – Type: doi
        Value: 10.1002/apj.2207
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      – Code: eng
        Text: English
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        PageCount: 11
        StartPage: 1
    Subjects:
      – SubjectFull: Solid oxide fuel cells
        Type: general
      – SubjectFull: Microwaves
        Type: general
      – SubjectFull: Iron ions
        Type: general
      – SubjectFull: Scanning electron microscopy
        Type: general
      – SubjectFull: X-ray diffraction
        Type: general
    Titles:
      – TitleFull: Synthesis of BaFe1‐xNixCuxO3‐δ new ceramic composition as solid oxide fuel cell cathode by microwave‐assisted solid‐state reaction.
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            NameFull: Moghaddas, Shahab
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            NameFull: Maghsoudipour, Amir
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            NameFull: Ebadzadeh, Touradj
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            – D: 01
              M: 07
              Text: Jul2018
              Type: published
              Y: 2018
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              Value: 13
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            – TitleFull: Asia-Pacific Journal of Chemical Engineering
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