Three-dimensional imaging and characterization of the oxide scale formed on a polycrystalline nickel-based superalloy.
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| Title: | Three-dimensional imaging and characterization of the oxide scale formed on a polycrystalline nickel-based superalloy. |
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| Authors: | Lech, Sebastian1 (AUTHOR) slech@agh.edu.pl, Kruk, Adam1 (AUTHOR), Gil, Aleksander1 (AUTHOR), Cempura, Grzegorz1 (AUTHOR), Agüero, Alina1 (AUTHOR), Czyrska-Filemonowicz, Aleksandra1 (AUTHOR) |
| Source: | Scripta Materialia. Jul2019, Vol. 167, p16-20. 5p. |
| Subjects: | Three-dimensional imaging, Scanning electron microscopes, Heat resistant alloys, Nickel alloys, Focused ion beams, Electron microscopy, Electron beams |
| Abstract: | Oxide scale formed on a polycrystalline nickel-based superalloy was investigated using analytical electron microscopy combined with three-dimensional tomography via conjunction of focused ion beam with scanning electron microscope. Application of these two complementary methods and correlation of the microscopy findings with three-dimensional imaging allowed to describe in detail the structure, chemistry, morphology and spatial distribution of phases and other structural elements formed during oxidation. An original approach proposed in our study allowed to identify the interlayer of the δ phase formed beneath the chromia scale and discuss formation of phases in the near-surface area and their role during oxidation. Unlabelled Image [ABSTRACT FROM AUTHOR] |
| Copyright of Scripta Materialia is the property of Pergamon Press - An Imprint of Elsevier Science and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.) | |
| Database: | Engineering Source |
| FullText | Text: Availability: 0 |
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| Header | DbId: egs DbLabel: Engineering Source An: 136070259 AccessLevel: 6 PubType: Academic Journal PubTypeId: academicJournal PreciseRelevancyScore: 0 |
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| Items | – Name: Title Label: Title Group: Ti Data: Three-dimensional imaging and characterization of the oxide scale formed on a polycrystalline nickel-based superalloy. – Name: Author Label: Authors Group: Au Data: <searchLink fieldCode="AR" term="%22Lech%2C+Sebastian%22">Lech, Sebastian</searchLink><relatesTo>1</relatesTo> (AUTHOR)<i> slech@agh.edu.pl</i><br /><searchLink fieldCode="AR" term="%22Kruk%2C+Adam%22">Kruk, Adam</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Gil%2C+Aleksander%22">Gil, Aleksander</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Cempura%2C+Grzegorz%22">Cempura, Grzegorz</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Agüero%2C+Alina%22">Agüero, Alina</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Czyrska-Filemonowicz%2C+Aleksandra%22">Czyrska-Filemonowicz, Aleksandra</searchLink><relatesTo>1</relatesTo> (AUTHOR) – Name: TitleSource Label: Source Group: Src Data: <searchLink fieldCode="JN" term="%22Scripta+Materialia%22">Scripta Materialia</searchLink>. Jul2019, Vol. 167, p16-20. 5p. – Name: Subject Label: Subjects Group: Su Data: <searchLink fieldCode="DE" term="%22Three-dimensional+imaging%22">Three-dimensional imaging</searchLink><br /><searchLink fieldCode="DE" term="%22Scanning+electron+microscopes%22">Scanning electron microscopes</searchLink><br /><searchLink fieldCode="DE" term="%22Heat+resistant+alloys%22">Heat resistant alloys</searchLink><br /><searchLink fieldCode="DE" term="%22Nickel+alloys%22">Nickel alloys</searchLink><br /><searchLink fieldCode="DE" term="%22Focused+ion+beams%22">Focused ion beams</searchLink><br /><searchLink fieldCode="DE" term="%22Electron+microscopy%22">Electron microscopy</searchLink><br /><searchLink fieldCode="DE" term="%22Electron+beams%22">Electron beams</searchLink> – Name: Abstract Label: Abstract Group: Ab Data: Oxide scale formed on a polycrystalline nickel-based superalloy was investigated using analytical electron microscopy combined with three-dimensional tomography via conjunction of focused ion beam with scanning electron microscope. Application of these two complementary methods and correlation of the microscopy findings with three-dimensional imaging allowed to describe in detail the structure, chemistry, morphology and spatial distribution of phases and other structural elements formed during oxidation. An original approach proposed in our study allowed to identify the interlayer of the δ phase formed beneath the chromia scale and discuss formation of phases in the near-surface area and their role during oxidation. Unlabelled Image [ABSTRACT FROM AUTHOR] – Name: AbstractSuppliedCopyright Label: Group: Ab Data: <i>Copyright of Scripta Materialia is the property of Pergamon Press - An Imprint of Elsevier Science and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.) |
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| RecordInfo | BibRecord: BibEntity: Identifiers: – Type: doi Value: 10.1016/j.scriptamat.2019.03.027 Languages: – Code: eng Text: English PhysicalDescription: Pagination: PageCount: 5 StartPage: 16 Subjects: – SubjectFull: Three-dimensional imaging Type: general – SubjectFull: Scanning electron microscopes Type: general – SubjectFull: Heat resistant alloys Type: general – SubjectFull: Nickel alloys Type: general – SubjectFull: Focused ion beams Type: general – SubjectFull: Electron microscopy Type: general – SubjectFull: Electron beams Type: general Titles: – TitleFull: Three-dimensional imaging and characterization of the oxide scale formed on a polycrystalline nickel-based superalloy. Type: main BibRelationships: HasContributorRelationships: – PersonEntity: Name: NameFull: Lech, Sebastian – PersonEntity: Name: NameFull: Kruk, Adam – PersonEntity: Name: NameFull: Gil, Aleksander – PersonEntity: Name: NameFull: Cempura, Grzegorz – PersonEntity: Name: NameFull: Agüero, Alina – PersonEntity: Name: NameFull: Czyrska-Filemonowicz, Aleksandra IsPartOfRelationships: – BibEntity: Dates: – D: 01 M: 07 Text: Jul2019 Type: published Y: 2019 Identifiers: – Type: issn-print Value: 13596462 Numbering: – Type: volume Value: 167 Titles: – TitleFull: Scripta Materialia Type: main |
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