Three-dimensional characterization of an oxide scale on ATI 718Plus® superalloy.

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Title: Three-dimensional characterization of an oxide scale on ATI 718Plus® superalloy.
Authors: Kruk, Adam1 (AUTHOR) kruczek@agh.edu.pl, Lech, Sebastian1 (AUTHOR) slech@agh.edu.pl, Gil, Aleksander2 (AUTHOR) gil@agh.edu.pl, Cempura, Grzegorz1 (AUTHOR) cempura@agh.edu.pl, Agüero, Alina3 (AUTHOR) agueroba@inta.es, Wusatowska-Sarnek, Agnieszka M.4 (AUTHOR) agnieszka.wusatowska-sarnek@prattwhitney.com, Czyrska-Filemonowicz, Aleksandra1 (AUTHOR) czyrska@agh.edu.pl
Source: Corrosion Science. Jun2020, Vol. 169, pN.PAG-N.PAG. 1p.
Subjects: Heat resistant alloys, Nickel-chromium alloys, Crystal grain boundaries, Chemistry, Oxides
Abstract: • FIB-SEM tomography supported by advanced TEM was an effective tool for 3D characterization of phases in oxidized 718Plus. • A discontinuous δ -Ni 3 Nb phase interlayer had formed directly underneath the Cr 2 O 3 scale. • Al 2 O 3 particles precipitated predominantly at grain boundaries. • Isolated chromia particles were present in the internal oxidation zone. • Nanosized γ phase precipitates enriched with Fe and Co were found within the Cr 2 O 3 scale. The presented study was devoted to the characterization of a scale formed on the ATI 718Plus® superalloy. Novel complementary techniques were applied to precisely describe the structure, chemistry, morphology of the scale as well as the spatial distribution of phases formed during oxidation. The study revealed a discontinuous interlayer of the δ -Ni 3 Nb phase that had developed underneath the protective Cr 2 O 3 scale. Al 2 O 3 particles, which had precipitated predominantly at grain boundaries, and isolated chromia particles were present in the internal oxidation zone. Nanosized γ phase precipitates enriched with Fe and Co were embedded into the scale. [ABSTRACT FROM AUTHOR]
Copyright of Corrosion Science is the property of Elsevier B.V. and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)
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  Data: Three-dimensional characterization of an oxide scale on ATI 718Plus® superalloy.
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  Data: <searchLink fieldCode="AR" term="%22Kruk%2C+Adam%22">Kruk, Adam</searchLink><relatesTo>1</relatesTo> (AUTHOR)<i> kruczek@agh.edu.pl</i><br /><searchLink fieldCode="AR" term="%22Lech%2C+Sebastian%22">Lech, Sebastian</searchLink><relatesTo>1</relatesTo> (AUTHOR)<i> slech@agh.edu.pl</i><br /><searchLink fieldCode="AR" term="%22Gil%2C+Aleksander%22">Gil, Aleksander</searchLink><relatesTo>2</relatesTo> (AUTHOR)<i> gil@agh.edu.pl</i><br /><searchLink fieldCode="AR" term="%22Cempura%2C+Grzegorz%22">Cempura, Grzegorz</searchLink><relatesTo>1</relatesTo> (AUTHOR)<i> cempura@agh.edu.pl</i><br /><searchLink fieldCode="AR" term="%22Agüero%2C+Alina%22">Agüero, Alina</searchLink><relatesTo>3</relatesTo> (AUTHOR)<i> agueroba@inta.es</i><br /><searchLink fieldCode="AR" term="%22Wusatowska-Sarnek%2C+Agnieszka+M%2E%22">Wusatowska-Sarnek, Agnieszka M.</searchLink><relatesTo>4</relatesTo> (AUTHOR)<i> agnieszka.wusatowska-sarnek@prattwhitney.com</i><br /><searchLink fieldCode="AR" term="%22Czyrska-Filemonowicz%2C+Aleksandra%22">Czyrska-Filemonowicz, Aleksandra</searchLink><relatesTo>1</relatesTo> (AUTHOR)<i> czyrska@agh.edu.pl</i>
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  Data: <searchLink fieldCode="JN" term="%22Corrosion+Science%22">Corrosion Science</searchLink>. Jun2020, Vol. 169, pN.PAG-N.PAG. 1p.
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  Data: <searchLink fieldCode="DE" term="%22Heat+resistant+alloys%22">Heat resistant alloys</searchLink><br /><searchLink fieldCode="DE" term="%22Nickel-chromium+alloys%22">Nickel-chromium alloys</searchLink><br /><searchLink fieldCode="DE" term="%22Crystal+grain+boundaries%22">Crystal grain boundaries</searchLink><br /><searchLink fieldCode="DE" term="%22Chemistry%22">Chemistry</searchLink><br /><searchLink fieldCode="DE" term="%22Oxides%22">Oxides</searchLink>
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  Data: • FIB-SEM tomography supported by advanced TEM was an effective tool for 3D characterization of phases in oxidized 718Plus. • A discontinuous δ -Ni 3 Nb phase interlayer had formed directly underneath the Cr 2 O 3 scale. • Al 2 O 3 particles precipitated predominantly at grain boundaries. • Isolated chromia particles were present in the internal oxidation zone. • Nanosized γ phase precipitates enriched with Fe and Co were found within the Cr 2 O 3 scale. The presented study was devoted to the characterization of a scale formed on the ATI 718Plus® superalloy. Novel complementary techniques were applied to precisely describe the structure, chemistry, morphology of the scale as well as the spatial distribution of phases formed during oxidation. The study revealed a discontinuous interlayer of the δ -Ni 3 Nb phase that had developed underneath the protective Cr 2 O 3 scale. Al 2 O 3 particles, which had precipitated predominantly at grain boundaries, and isolated chromia particles were present in the internal oxidation zone. Nanosized γ phase precipitates enriched with Fe and Co were embedded into the scale. [ABSTRACT FROM AUTHOR]
– Name: AbstractSuppliedCopyright
  Label:
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  Data: <i>Copyright of Corrosion Science is the property of Elsevier B.V. and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.)
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      – Type: doi
        Value: 10.1016/j.corsci.2020.108634
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        Text: English
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      – SubjectFull: Heat resistant alloys
        Type: general
      – SubjectFull: Nickel-chromium alloys
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      – SubjectFull: Crystal grain boundaries
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      – SubjectFull: Chemistry
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      – SubjectFull: Oxides
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      – TitleFull: Three-dimensional characterization of an oxide scale on ATI 718Plus® superalloy.
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              Text: Jun2020
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              Y: 2020
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