Specific adsorption of tetracycline from milk by using biocompatible magnetic molecular imprinting material and evaluation by ECD.
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| Title: | Specific adsorption of tetracycline from milk by using biocompatible magnetic molecular imprinting material and evaluation by ECD. |
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| Authors: | Wang, Shu-Xian1 (AUTHOR), Ma, Rong-Rong1 (AUTHOR), Mazzu, Ying Z.2 (AUTHOR), Zhang, Jia-Wei1 (AUTHOR), Li, Wei1 (AUTHOR), Tan, Ling1 (AUTHOR), Zhou, Lian-Di1,3 (AUTHOR) 102501@cqmu.edu.cn, Xia, Zhi-Ning1 (AUTHOR), Zhang, Qi-Hui1,2 (AUTHOR) qhzhang@cqu.edu.cn, Yuan, Chun-Su4 (AUTHOR) |
| Source: | Food Chemistry. Oct2020, Vol. 326, pN.PAG-N.PAG. 1p. |
| Subjects: | Tetracyclines, Tetracycline, Molecular imprinting, Transmission electron microscopes, Imprinted polymers, Scanning electron microscopes, Langmuir isotherms |
| Abstract: | • BMMIPs possess biocompatibility and specific adsorption capacity for tetracycline. • Zein is an optimal choice for the raw material of BMMIPs. • The application of BMMIPs combined with ECD is valuable for practical application. Biocompatible magnetic molecularly imprinted polymers (BMMIPs) were prepared with Zein for the first time, and were used to enrich tetracycline compounds selectively. Innovative combination of BMMIPs and electrochemistry to obtain lower detection line to satisfy industrial detection demands. Using Zein as the crosslinking agent, the polymers were synthesized on the surface of Fe 3 O 4 particles. The scanning electron microscope, transmission electron microscope and X-ray diffraction technologies were used to characterize BMMIPs. Through optimization, BMMIPs attained large adsorption capacity (236.40 mg/g) with fast kinetics (40 min) and followed the Langmuir isotherm and pseudo-second-order kinetic models. BMMIPs had good recognition ability, the selective factors of oxytetracycline, chlortetracycline, doxycycline were 4.78, 4.23, and 3.39, respectively. Excellent linearity was attained in the range of 0.025–500 μg/mL, with low detection limits and low quantitation limits of 0.025 and 0.083 μg/mL. According to our exploring, BMMIPs was ideal materials for enrichment of tetracycline in complex biological samples. [ABSTRACT FROM AUTHOR] |
| Copyright of Food Chemistry is the property of Elsevier B.V. and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.) | |
| Database: | Engineering Source |
| FullText | Text: Availability: 0 |
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| Header | DbId: egs DbLabel: Engineering Source An: 143555467 AccessLevel: 6 PubType: Academic Journal PubTypeId: academicJournal PreciseRelevancyScore: 0 |
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| Items | – Name: Title Label: Title Group: Ti Data: Specific adsorption of tetracycline from milk by using biocompatible magnetic molecular imprinting material and evaluation by ECD. – Name: Author Label: Authors Group: Au Data: <searchLink fieldCode="AR" term="%22Wang%2C+Shu-Xian%22">Wang, Shu-Xian</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Ma%2C+Rong-Rong%22">Ma, Rong-Rong</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Mazzu%2C+Ying+Z%2E%22">Mazzu, Ying Z.</searchLink><relatesTo>2</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Zhang%2C+Jia-Wei%22">Zhang, Jia-Wei</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Li%2C+Wei%22">Li, Wei</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Tan%2C+Ling%22">Tan, Ling</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Zhou%2C+Lian-Di%22">Zhou, Lian-Di</searchLink><relatesTo>1,3</relatesTo> (AUTHOR)<i> 102501@cqmu.edu.cn</i><br /><searchLink fieldCode="AR" term="%22Xia%2C+Zhi-Ning%22">Xia, Zhi-Ning</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Zhang%2C+Qi-Hui%22">Zhang, Qi-Hui</searchLink><relatesTo>1,2</relatesTo> (AUTHOR)<i> qhzhang@cqu.edu.cn</i><br /><searchLink fieldCode="AR" term="%22Yuan%2C+Chun-Su%22">Yuan, Chun-Su</searchLink><relatesTo>4</relatesTo> (AUTHOR) – Name: TitleSource Label: Source Group: Src Data: <searchLink fieldCode="JN" term="%22Food+Chemistry%22">Food Chemistry</searchLink>. Oct2020, Vol. 326, pN.PAG-N.PAG. 1p. – Name: Subject Label: Subjects Group: Su Data: <searchLink fieldCode="DE" term="%22Tetracyclines%22">Tetracyclines</searchLink><br /><searchLink fieldCode="DE" term="%22Tetracycline%22">Tetracycline</searchLink><br /><searchLink fieldCode="DE" term="%22Molecular+imprinting%22">Molecular imprinting</searchLink><br /><searchLink fieldCode="DE" term="%22Transmission+electron+microscopes%22">Transmission electron microscopes</searchLink><br /><searchLink fieldCode="DE" term="%22Imprinted+polymers%22">Imprinted polymers</searchLink><br /><searchLink fieldCode="DE" term="%22Scanning+electron+microscopes%22">Scanning electron microscopes</searchLink><br /><searchLink fieldCode="DE" term="%22Langmuir+isotherms%22">Langmuir isotherms</searchLink> – Name: Abstract Label: Abstract Group: Ab Data: • BMMIPs possess biocompatibility and specific adsorption capacity for tetracycline. • Zein is an optimal choice for the raw material of BMMIPs. • The application of BMMIPs combined with ECD is valuable for practical application. Biocompatible magnetic molecularly imprinted polymers (BMMIPs) were prepared with Zein for the first time, and were used to enrich tetracycline compounds selectively. Innovative combination of BMMIPs and electrochemistry to obtain lower detection line to satisfy industrial detection demands. Using Zein as the crosslinking agent, the polymers were synthesized on the surface of Fe 3 O 4 particles. The scanning electron microscope, transmission electron microscope and X-ray diffraction technologies were used to characterize BMMIPs. Through optimization, BMMIPs attained large adsorption capacity (236.40 mg/g) with fast kinetics (40 min) and followed the Langmuir isotherm and pseudo-second-order kinetic models. BMMIPs had good recognition ability, the selective factors of oxytetracycline, chlortetracycline, doxycycline were 4.78, 4.23, and 3.39, respectively. Excellent linearity was attained in the range of 0.025–500 μg/mL, with low detection limits and low quantitation limits of 0.025 and 0.083 μg/mL. According to our exploring, BMMIPs was ideal materials for enrichment of tetracycline in complex biological samples. [ABSTRACT FROM AUTHOR] – Name: AbstractSuppliedCopyright Label: Group: Ab Data: <i>Copyright of Food Chemistry is the property of Elsevier B.V. and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.) |
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| RecordInfo | BibRecord: BibEntity: Identifiers: – Type: doi Value: 10.1016/j.foodchem.2020.126969 Languages: – Code: eng Text: English PhysicalDescription: Pagination: PageCount: 1 StartPage: N.PAG Subjects: – SubjectFull: Tetracyclines Type: general – SubjectFull: Tetracycline Type: general – SubjectFull: Molecular imprinting Type: general – SubjectFull: Transmission electron microscopes Type: general – SubjectFull: Imprinted polymers Type: general – SubjectFull: Scanning electron microscopes Type: general – SubjectFull: Langmuir isotherms Type: general Titles: – TitleFull: Specific adsorption of tetracycline from milk by using biocompatible magnetic molecular imprinting material and evaluation by ECD. Type: main BibRelationships: HasContributorRelationships: – PersonEntity: Name: NameFull: Wang, Shu-Xian – PersonEntity: Name: NameFull: Ma, Rong-Rong – PersonEntity: Name: NameFull: Mazzu, Ying Z. – PersonEntity: Name: NameFull: Zhang, Jia-Wei – PersonEntity: Name: NameFull: Li, Wei – PersonEntity: Name: NameFull: Tan, Ling – PersonEntity: Name: NameFull: Zhou, Lian-Di – PersonEntity: Name: NameFull: Xia, Zhi-Ning – PersonEntity: Name: NameFull: Zhang, Qi-Hui – PersonEntity: Name: NameFull: Yuan, Chun-Su IsPartOfRelationships: – BibEntity: Dates: – D: 01 M: 10 Text: Oct2020 Type: published Y: 2020 Identifiers: – Type: issn-print Value: 03088146 Numbering: – Type: volume Value: 326 Titles: – TitleFull: Food Chemistry Type: main |
| ResultId | 1 |