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An original concept for the synthesis of an oxide coating: The film boiling process.

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Title: An original concept for the synthesis of an oxide coating: The film boiling process.
Authors: Besnard, C.1 (AUTHOR), Allemand, A.1,2 (AUTHOR), David, P.2 (AUTHOR), Léon, J.F.3 (AUTHOR), Maillé, L.1 (AUTHOR) maille@lcts.u-bordeaux.fr
Source: Journal of the European Ceramic Society. May2021, Vol. 41 Issue 5, p3013-3018. 6p.
Subjects: Oxide coating, Electron probe microanalysis, Ceramic coating, Composite coating, Ebullition, Anthology films
Abstract: The film boiling chemical vapor process is an original and rapid synthesis method for ceramic coatings and composites. This work reports the deposition of silica coating from tetraethyl orthosilicate (TEOS) by film boiling chemical vapor process. Experiments were carried out under atmospheric pressure between 900 °C and 1100 °C. Several modifications of the experimental setup were made in order to allow a better thermal monitoring. Silica coatings were fast synthetized: several microns per minute. An activation energy of 209 kJ/mol ± 20 was deduced. The structure and microstructure of the oxide coating were characterized by Optical Microscopy, Scanning Electron Microscopy, Energy Dispersive Spectroscopy, Electron Probe MicroAnalyzer, Fourier-Transform InfraRed spectrometery and X-ray diffraction. [ABSTRACT FROM AUTHOR]
Copyright of Journal of the European Ceramic Society is the property of Elsevier B.V. and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)
Database: Engineering Source
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  Availability: 0
Header DbId: egs
DbLabel: Engineering Source
An: 148732558
AccessLevel: 6
PubType: Academic Journal
PubTypeId: academicJournal
PreciseRelevancyScore: 0
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  Data: An original concept for the synthesis of an oxide coating: The film boiling process.
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  Data: <searchLink fieldCode="AR" term="%22Besnard%2C+C%2E%22">Besnard, C.</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Allemand%2C+A%2E%22">Allemand, A.</searchLink><relatesTo>1,2</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22David%2C+P%2E%22">David, P.</searchLink><relatesTo>2</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Léon%2C+J%2EF%2E%22">Léon, J.F.</searchLink><relatesTo>3</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Maillé%2C+L%2E%22">Maillé, L.</searchLink><relatesTo>1</relatesTo> (AUTHOR)<i> maille@lcts.u-bordeaux.fr</i>
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  Data: <searchLink fieldCode="JN" term="%22Journal+of+the+European+Ceramic+Society%22">Journal of the European Ceramic Society</searchLink>. May2021, Vol. 41 Issue 5, p3013-3018. 6p.
– Name: Subject
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  Data: <searchLink fieldCode="DE" term="%22Oxide+coating%22">Oxide coating</searchLink><br /><searchLink fieldCode="DE" term="%22Electron+probe+microanalysis%22">Electron probe microanalysis</searchLink><br /><searchLink fieldCode="DE" term="%22Ceramic+coating%22">Ceramic coating</searchLink><br /><searchLink fieldCode="DE" term="%22Composite+coating%22">Composite coating</searchLink><br /><searchLink fieldCode="DE" term="%22Ebullition%22">Ebullition</searchLink><br /><searchLink fieldCode="DE" term="%22Anthology+films%22">Anthology films</searchLink>
– Name: Abstract
  Label: Abstract
  Group: Ab
  Data: The film boiling chemical vapor process is an original and rapid synthesis method for ceramic coatings and composites. This work reports the deposition of silica coating from tetraethyl orthosilicate (TEOS) by film boiling chemical vapor process. Experiments were carried out under atmospheric pressure between 900 °C and 1100 °C. Several modifications of the experimental setup were made in order to allow a better thermal monitoring. Silica coatings were fast synthetized: several microns per minute. An activation energy of 209 kJ/mol ± 20 was deduced. The structure and microstructure of the oxide coating were characterized by Optical Microscopy, Scanning Electron Microscopy, Energy Dispersive Spectroscopy, Electron Probe MicroAnalyzer, Fourier-Transform InfraRed spectrometery and X-ray diffraction. [ABSTRACT FROM AUTHOR]
– Name: AbstractSuppliedCopyright
  Label:
  Group: Ab
  Data: <i>Copyright of Journal of the European Ceramic Society is the property of Elsevier B.V. and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.)
PLink https://search.ebscohost.com/login.aspx?direct=true&site=eds-live&db=egs&AN=148732558
RecordInfo BibRecord:
  BibEntity:
    Identifiers:
      – Type: doi
        Value: 10.1016/j.jeurceramsoc.2020.10.069
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      – Code: eng
        Text: English
    PhysicalDescription:
      Pagination:
        PageCount: 6
        StartPage: 3013
    Subjects:
      – SubjectFull: Oxide coating
        Type: general
      – SubjectFull: Electron probe microanalysis
        Type: general
      – SubjectFull: Ceramic coating
        Type: general
      – SubjectFull: Composite coating
        Type: general
      – SubjectFull: Ebullition
        Type: general
      – SubjectFull: Anthology films
        Type: general
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      – TitleFull: An original concept for the synthesis of an oxide coating: The film boiling process.
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            NameFull: Besnard, C.
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            NameFull: Allemand, A.
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            NameFull: David, P.
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            NameFull: Léon, J.F.
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            NameFull: Maillé, L.
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            – D: 01
              M: 05
              Text: May2021
              Type: published
              Y: 2021
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              Value: 41
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            – TitleFull: Journal of the European Ceramic Society
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