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Facile synthesis and characterization of polymerizable tertiary amines.

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Title: Facile synthesis and characterization of polymerizable tertiary amines.
Authors: Sun, Qiujie1 (AUTHOR), Dong, Ping1 (AUTHOR), Fan, Yi1 (AUTHOR), Han, Yuxuan1 (AUTHOR), Huang, Wenyan1 (AUTHOR) ellahwy@cczu.edu.cn, Jiang, Li1 (AUTHOR), Jiang, Qimin1 (AUTHOR), Xue, Xiaoqiang1 (AUTHOR), Yang, Hongjun1 (AUTHOR), Jiang, Bibiao1 (AUTHOR) jiangbibiao@cczu.edu.cn
Source: Materials Research Innovations. Jun2021, Vol. 25 Issue 4, p249-256. 8p.
Subjects: Tertiary amines, Proton magnetic resonance, Chemical synthesis, Acrylamide, Nuclear magnetic resonance, Acyl chlorides, Tertiary structure
Abstract: Tertiary amine-structured compounds containing stimulating response groups such as diethylaminoethyl isobutyrate and N-(2-(dimethylamino)ethyl)methyl, were synthesised by an acid chloride esterification method using acrylamide, N-(2-(dimethylamino) ethyl)isobutyramide, 2-methyl-N-[3-(methyl-phenyl-amino)-propyl]-acrylamide and 2-Methyl -N-[3-(methyl-phenyl-amino)-propyl]-propionamide reactants. The effects of different ratios of reactants on product purity, reaction time on purity and yield were investigated. Product purity was characterised by gas chromatography. The structure was characterised by infrared spectroscopy (IR) and proton nuclear magnetic resonance (1H-NMR), and the purity of the five different synthesised compounds was determined to be more than 97%. This study provides a convenient and efficient method for the synthesis of compounds containing tertiary amine structures. [ABSTRACT FROM AUTHOR]
Copyright of Materials Research Innovations is the property of Taylor & Francis Ltd and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)
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An: 150470866
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PubTypeId: academicJournal
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  Data: Facile synthesis and characterization of polymerizable tertiary amines.
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  Data: <searchLink fieldCode="AR" term="%22Sun%2C+Qiujie%22">Sun, Qiujie</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Dong%2C+Ping%22">Dong, Ping</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Fan%2C+Yi%22">Fan, Yi</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Han%2C+Yuxuan%22">Han, Yuxuan</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Huang%2C+Wenyan%22">Huang, Wenyan</searchLink><relatesTo>1</relatesTo> (AUTHOR)<i> ellahwy@cczu.edu.cn</i><br /><searchLink fieldCode="AR" term="%22Jiang%2C+Li%22">Jiang, Li</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Jiang%2C+Qimin%22">Jiang, Qimin</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Xue%2C+Xiaoqiang%22">Xue, Xiaoqiang</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Yang%2C+Hongjun%22">Yang, Hongjun</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Jiang%2C+Bibiao%22">Jiang, Bibiao</searchLink><relatesTo>1</relatesTo> (AUTHOR)<i> jiangbibiao@cczu.edu.cn</i>
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  Data: <searchLink fieldCode="JN" term="%22Materials+Research+Innovations%22">Materials Research Innovations</searchLink>. Jun2021, Vol. 25 Issue 4, p249-256. 8p.
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  Data: <searchLink fieldCode="DE" term="%22Tertiary+amines%22">Tertiary amines</searchLink><br /><searchLink fieldCode="DE" term="%22Proton+magnetic+resonance%22">Proton magnetic resonance</searchLink><br /><searchLink fieldCode="DE" term="%22Chemical+synthesis%22">Chemical synthesis</searchLink><br /><searchLink fieldCode="DE" term="%22Acrylamide%22">Acrylamide</searchLink><br /><searchLink fieldCode="DE" term="%22Nuclear+magnetic+resonance%22">Nuclear magnetic resonance</searchLink><br /><searchLink fieldCode="DE" term="%22Acyl+chlorides%22">Acyl chlorides</searchLink><br /><searchLink fieldCode="DE" term="%22Tertiary+structure%22">Tertiary structure</searchLink>
– Name: Abstract
  Label: Abstract
  Group: Ab
  Data: Tertiary amine-structured compounds containing stimulating response groups such as diethylaminoethyl isobutyrate and N-(2-(dimethylamino)ethyl)methyl, were synthesised by an acid chloride esterification method using acrylamide, N-(2-(dimethylamino) ethyl)isobutyramide, 2-methyl-N-[3-(methyl-phenyl-amino)-propyl]-acrylamide and 2-Methyl -N-[3-(methyl-phenyl-amino)-propyl]-propionamide reactants. The effects of different ratios of reactants on product purity, reaction time on purity and yield were investigated. Product purity was characterised by gas chromatography. The structure was characterised by infrared spectroscopy (IR) and proton nuclear magnetic resonance (1H-NMR), and the purity of the five different synthesised compounds was determined to be more than 97%. This study provides a convenient and efficient method for the synthesis of compounds containing tertiary amine structures. [ABSTRACT FROM AUTHOR]
– Name: AbstractSuppliedCopyright
  Label:
  Group: Ab
  Data: <i>Copyright of Materials Research Innovations is the property of Taylor & Francis Ltd and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.)
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RecordInfo BibRecord:
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      – Type: doi
        Value: 10.1080/14328917.2021.1926073
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      – Code: eng
        Text: English
    PhysicalDescription:
      Pagination:
        PageCount: 8
        StartPage: 249
    Subjects:
      – SubjectFull: Tertiary amines
        Type: general
      – SubjectFull: Proton magnetic resonance
        Type: general
      – SubjectFull: Chemical synthesis
        Type: general
      – SubjectFull: Acrylamide
        Type: general
      – SubjectFull: Nuclear magnetic resonance
        Type: general
      – SubjectFull: Acyl chlorides
        Type: general
      – SubjectFull: Tertiary structure
        Type: general
    Titles:
      – TitleFull: Facile synthesis and characterization of polymerizable tertiary amines.
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            NameFull: Sun, Qiujie
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            NameFull: Dong, Ping
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            – D: 01
              M: 06
              Text: Jun2021
              Type: published
              Y: 2021
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