Observation of Peek Melting Peaks within the Additive Manufacturing Material Extrusion Process in Relation to Isothermal and Non‐Isothermal Processes.
Saved in:
| Title: | Observation of Peek Melting Peaks within the Additive Manufacturing Material Extrusion Process in Relation to Isothermal and Non‐Isothermal Processes. |
|---|---|
| Authors: | Comelli, Cleiton André1 (AUTHOR) c.a.comelli@exeter.ac.uk, Yi, Nan1 (AUTHOR), Davies, Richard1 (AUTHOR), van der Pol, HenkJan2 (AUTHOR), Ghita, Oana1 (AUTHOR) |
| Source: | Macromolecular Materials & Engineering. Apr2024, Vol. 309 Issue 4, p1-17. 17p. |
| Subjects: | Extrusion process, Isothermal processes, Manufacturing processes, Plastic extrusion, Differential scanning calorimetry, Isothermal temperature, Melting |
| Abstract: | The current study investigates the melting behavior of polyetheretherketone (PEEK) using both Differential Scanning Calorimetry (DSC) and Fast Scanning Calorimetry (FSC) thermal analysis techniques. The PEEK melting peaks are examined under various conditions, including isothermal and non‐isothermal crystallization conditions, as well as a thermal profile mimicking the material extrusion process (MEX). The results of the analysis reveal changes in the crystalline morphology, as indicated by a shift in intensity between melting peaks crystalized at different isothermal temperatures and cooling rates. Furthermore, the behavior of the deconvoluted melting peaks differs depending on the substrate temperature during the MEX process simulation. The presence of double or multiple melting peaks suggests the presence of different crystalline populations during the manufacturing process. Understanding the formation and changes in these melting peaks can help inform the development of better printing strategies and improve the mechanical performance of printed parts. [ABSTRACT FROM AUTHOR] |
| Copyright of Macromolecular Materials & Engineering is the property of Wiley-Blackwell and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.) | |
| Database: | Engineering Source |
|
Full text is not displayed to guests.
Login for full access.
|
|
| FullText | Links: – Type: pdflink Text: Availability: 1 |
|---|---|
| Header | DbId: egs DbLabel: Engineering Source An: 176608382 AccessLevel: 6 PubType: Academic Journal PubTypeId: academicJournal PreciseRelevancyScore: 0 |
| IllustrationInfo | |
| Items | – Name: Title Label: Title Group: Ti Data: Observation of Peek Melting Peaks within the Additive Manufacturing Material Extrusion Process in Relation to Isothermal and Non‐Isothermal Processes. – Name: Author Label: Authors Group: Au Data: <searchLink fieldCode="AR" term="%22Comelli%2C+Cleiton+André%22">Comelli, Cleiton André</searchLink><relatesTo>1</relatesTo> (AUTHOR)<i> c.a.comelli@exeter.ac.uk</i><br /><searchLink fieldCode="AR" term="%22Yi%2C+Nan%22">Yi, Nan</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Davies%2C+Richard%22">Davies, Richard</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22van+der+Pol%2C+HenkJan%22">van der Pol, HenkJan</searchLink><relatesTo>2</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Ghita%2C+Oana%22">Ghita, Oana</searchLink><relatesTo>1</relatesTo> (AUTHOR) – Name: TitleSource Label: Source Group: Src Data: <searchLink fieldCode="JN" term="%22Macromolecular+Materials+%26+Engineering%22">Macromolecular Materials & Engineering</searchLink>. Apr2024, Vol. 309 Issue 4, p1-17. 17p. – Name: Subject Label: Subjects Group: Su Data: <searchLink fieldCode="DE" term="%22Extrusion+process%22">Extrusion process</searchLink><br /><searchLink fieldCode="DE" term="%22Isothermal+processes%22">Isothermal processes</searchLink><br /><searchLink fieldCode="DE" term="%22Manufacturing+processes%22">Manufacturing processes</searchLink><br /><searchLink fieldCode="DE" term="%22Plastic+extrusion%22">Plastic extrusion</searchLink><br /><searchLink fieldCode="DE" term="%22Differential+scanning+calorimetry%22">Differential scanning calorimetry</searchLink><br /><searchLink fieldCode="DE" term="%22Isothermal+temperature%22">Isothermal temperature</searchLink><br /><searchLink fieldCode="DE" term="%22Melting%22">Melting</searchLink> – Name: Abstract Label: Abstract Group: Ab Data: The current study investigates the melting behavior of polyetheretherketone (PEEK) using both Differential Scanning Calorimetry (DSC) and Fast Scanning Calorimetry (FSC) thermal analysis techniques. The PEEK melting peaks are examined under various conditions, including isothermal and non‐isothermal crystallization conditions, as well as a thermal profile mimicking the material extrusion process (MEX). The results of the analysis reveal changes in the crystalline morphology, as indicated by a shift in intensity between melting peaks crystalized at different isothermal temperatures and cooling rates. Furthermore, the behavior of the deconvoluted melting peaks differs depending on the substrate temperature during the MEX process simulation. The presence of double or multiple melting peaks suggests the presence of different crystalline populations during the manufacturing process. Understanding the formation and changes in these melting peaks can help inform the development of better printing strategies and improve the mechanical performance of printed parts. [ABSTRACT FROM AUTHOR] – Name: AbstractSuppliedCopyright Label: Group: Ab Data: <i>Copyright of Macromolecular Materials & Engineering is the property of Wiley-Blackwell and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.) |
| PLink | https://search.ebscohost.com/login.aspx?direct=true&site=eds-live&db=egs&AN=176608382 |
| RecordInfo | BibRecord: BibEntity: Identifiers: – Type: doi Value: 10.1002/mame.202300386 Languages: – Code: eng Text: English PhysicalDescription: Pagination: PageCount: 17 StartPage: 1 Subjects: – SubjectFull: Extrusion process Type: general – SubjectFull: Isothermal processes Type: general – SubjectFull: Manufacturing processes Type: general – SubjectFull: Plastic extrusion Type: general – SubjectFull: Differential scanning calorimetry Type: general – SubjectFull: Isothermal temperature Type: general – SubjectFull: Melting Type: general Titles: – TitleFull: Observation of Peek Melting Peaks within the Additive Manufacturing Material Extrusion Process in Relation to Isothermal and Non‐Isothermal Processes. Type: main BibRelationships: HasContributorRelationships: – PersonEntity: Name: NameFull: Comelli, Cleiton André – PersonEntity: Name: NameFull: Yi, Nan – PersonEntity: Name: NameFull: Davies, Richard – PersonEntity: Name: NameFull: van der Pol, HenkJan – PersonEntity: Name: NameFull: Ghita, Oana IsPartOfRelationships: – BibEntity: Dates: – D: 01 M: 04 Text: Apr2024 Type: published Y: 2024 Identifiers: – Type: issn-print Value: 14387492 Numbering: – Type: volume Value: 309 – Type: issue Value: 4 Titles: – TitleFull: Macromolecular Materials & Engineering Type: main |
| ResultId | 1 |
