Preparation, Structural, and Magnetic Properties of Soft (Ni0.6Zn0.4Fe2O4) and Hard (BaFe12O19) Ferrite Composites.

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Title: Preparation, Structural, and Magnetic Properties of Soft (Ni0.6Zn0.4Fe2O4) and Hard (BaFe12O19) Ferrite Composites.
Authors: Ramesh, T.1 (AUTHOR) rameshouphysics@gmail.com, Usha, P.2 (AUTHOR), Venkatesh, D.3 (AUTHOR), Sadhana, K.4 (AUTHOR), Praveena, K.5 (AUTHOR), Ashok, K.6 (AUTHOR) kolluashok11@gmail.com
Source: Journal of Superconductivity & Novel Magnetism. Oct2024, Vol. 37 Issue 8-10, p1617-1628. 12p.
Subjects: Field emission electron microscopy, Heat treatment, Magnetic properties, Hysteresis loop, Band gaps
Abstract: Barium hexaferrite (BaFe12O19) and Ni–Zn ferrite (Ni0.6Zn0.4Fe2O4) powders were synthesized using the microwave hydrothermal method. Composite samples with varying ratios {x(Ni0.6Zn0.4Fe2O4) + (1 − x) (BaFe12O19)} (where x ranged from 0 to 1.0) were prepared through mechanical mixing. The pure and composite samples were subjected to a 4-h heat treatment at 800 °C. The structural characteristics of the pure samples were analyzed using X-ray diffraction (XRD), revealing the hexagonal structure of BaFe12O19 and the spinel structure of Ni0.6Zn0.4Fe2O4. Morphological properties were investigated using field emission scanning electron microscopy (FESEM). The results confirmed a hexagonal morphology for BaFe12O19, a spherical morphology for Ni0.6Zn0.4Fe2O4, and a mixed morphology for the composites, with grain sizes ranging from 50 to 200 nm. The optical properties were explored through UV–Vis absorption studies, and the optical energy gap values were determined using the Tauc plots. The magnetic behavior of the samples was studied by analyzing magnetic hysteresis loops. Pure samples exhibited a smooth hysteresis behavior, while composite samples displayed a step-like pattern. A possible relation between the magnetic interaction between the two different materials in the composites was investigated. [ABSTRACT FROM AUTHOR]
Copyright of Journal of Superconductivity & Novel Magnetism is the property of Springer Nature and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)
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  Data: Preparation, Structural, and Magnetic Properties of Soft (Ni<subscript>0.6</subscript>Zn<subscript>0.4</subscript>Fe<subscript>2</subscript>O<subscript>4</subscript>) and Hard (BaFe<subscript>12</subscript>O<subscript>19</subscript>) Ferrite Composites.
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  Data: <searchLink fieldCode="AR" term="%22Ramesh%2C+T%2E%22">Ramesh, T.</searchLink><relatesTo>1</relatesTo> (AUTHOR)<i> rameshouphysics@gmail.com</i><br /><searchLink fieldCode="AR" term="%22Usha%2C+P%2E%22">Usha, P.</searchLink><relatesTo>2</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Venkatesh%2C+D%2E%22">Venkatesh, D.</searchLink><relatesTo>3</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Sadhana%2C+K%2E%22">Sadhana, K.</searchLink><relatesTo>4</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Praveena%2C+K%2E%22">Praveena, K.</searchLink><relatesTo>5</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Ashok%2C+K%2E%22">Ashok, K.</searchLink><relatesTo>6</relatesTo> (AUTHOR)<i> kolluashok11@gmail.com</i>
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  Data: <searchLink fieldCode="JN" term="%22Journal+of+Superconductivity+%26+Novel+Magnetism%22">Journal of Superconductivity & Novel Magnetism</searchLink>. Oct2024, Vol. 37 Issue 8-10, p1617-1628. 12p.
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  Data: <searchLink fieldCode="DE" term="%22Field+emission+electron+microscopy%22">Field emission electron microscopy</searchLink><br /><searchLink fieldCode="DE" term="%22Heat+treatment%22">Heat treatment</searchLink><br /><searchLink fieldCode="DE" term="%22Magnetic+properties%22">Magnetic properties</searchLink><br /><searchLink fieldCode="DE" term="%22Hysteresis+loop%22">Hysteresis loop</searchLink><br /><searchLink fieldCode="DE" term="%22Band+gaps%22">Band gaps</searchLink>
– Name: Abstract
  Label: Abstract
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  Data: Barium hexaferrite (BaFe12O19) and Ni–Zn ferrite (Ni0.6Zn0.4Fe2O4) powders were synthesized using the microwave hydrothermal method. Composite samples with varying ratios {x(Ni0.6Zn0.4Fe2O4) + (1 − x) (BaFe12O19)} (where x ranged from 0 to 1.0) were prepared through mechanical mixing. The pure and composite samples were subjected to a 4-h heat treatment at 800 °C. The structural characteristics of the pure samples were analyzed using X-ray diffraction (XRD), revealing the hexagonal structure of BaFe12O19 and the spinel structure of Ni0.6Zn0.4Fe2O4. Morphological properties were investigated using field emission scanning electron microscopy (FESEM). The results confirmed a hexagonal morphology for BaFe12O19, a spherical morphology for Ni0.6Zn0.4Fe2O4, and a mixed morphology for the composites, with grain sizes ranging from 50 to 200 nm. The optical properties were explored through UV–Vis absorption studies, and the optical energy gap values were determined using the Tauc plots. The magnetic behavior of the samples was studied by analyzing magnetic hysteresis loops. Pure samples exhibited a smooth hysteresis behavior, while composite samples displayed a step-like pattern. A possible relation between the magnetic interaction between the two different materials in the composites was investigated. [ABSTRACT FROM AUTHOR]
– Name: AbstractSuppliedCopyright
  Label:
  Group: Ab
  Data: <i>Copyright of Journal of Superconductivity & Novel Magnetism is the property of Springer Nature and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.)
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        Value: 10.1007/s10948-024-06794-7
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        Text: English
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      – SubjectFull: Field emission electron microscopy
        Type: general
      – SubjectFull: Heat treatment
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      – SubjectFull: Magnetic properties
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      – SubjectFull: Hysteresis loop
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      – SubjectFull: Band gaps
        Type: general
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      – TitleFull: Preparation, Structural, and Magnetic Properties of Soft (Ni0.6Zn0.4Fe2O4) and Hard (BaFe12O19) Ferrite Composites.
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              M: 10
              Text: Oct2024
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