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Tutorial for thermal analysis of ionic liquids.

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Title: Tutorial for thermal analysis of ionic liquids.
Authors: Papović, Snežana1 (AUTHOR), Vraneš, Milan1 (AUTHOR), Barta Holló, Berta1 (AUTHOR), Mészáros Szécsényi, Katalin1 (AUTHOR) mszk@uns.ac.rs
Source: Journal of Thermal Analysis & Calorimetry. Oct2024, Vol. 149 Issue 20, p11407-11419. 13p.
Subjects: Liquid analysis, Ionic liquids, Debye temperatures, Thermal analysis, Data visualization
Abstract: This tutorial aims to show the basic steps of evaluating the thermoanalytical curves to obtain reliable data for comparison with literature data for ionic liquids (ILs). The thermoanalytical investigation of the series of bis(trifluoromethylsulfonyl)imide-based imidazolium derivatives is described. The effects of the experimental conditions, such as the atmosphere and sample pan type, on the results, are outlined. The determination of the characteristic temperatures of the decomposition is described. The difficulties in obtaining reliable data for comparison are highlighted. The advantages of applying the simultaneous TG–DSC technique are shown by comparing the corresponding derivative DTG and DSC curves. Examples of the visualization and evaluation of the data of the compound series are presented. The results of the hyphenated TG–MS measurements are evaluated. The limitations of the applied techniques are discussed, too. The principles of here described evaluation steps of the thermoanalytical curves can be generally applied not only to ILs but to most of the sample types. [ABSTRACT FROM AUTHOR]
Copyright of Journal of Thermal Analysis & Calorimetry is the property of Springer Nature and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)
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  Data: <searchLink fieldCode="DE" term="%22Liquid+analysis%22">Liquid analysis</searchLink><br /><searchLink fieldCode="DE" term="%22Ionic+liquids%22">Ionic liquids</searchLink><br /><searchLink fieldCode="DE" term="%22Debye+temperatures%22">Debye temperatures</searchLink><br /><searchLink fieldCode="DE" term="%22Thermal+analysis%22">Thermal analysis</searchLink><br /><searchLink fieldCode="DE" term="%22Data+visualization%22">Data visualization</searchLink>
– Name: Abstract
  Label: Abstract
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  Data: This tutorial aims to show the basic steps of evaluating the thermoanalytical curves to obtain reliable data for comparison with literature data for ionic liquids (ILs). The thermoanalytical investigation of the series of bis(trifluoromethylsulfonyl)imide-based imidazolium derivatives is described. The effects of the experimental conditions, such as the atmosphere and sample pan type, on the results, are outlined. The determination of the characteristic temperatures of the decomposition is described. The difficulties in obtaining reliable data for comparison are highlighted. The advantages of applying the simultaneous TG–DSC technique are shown by comparing the corresponding derivative DTG and DSC curves. Examples of the visualization and evaluation of the data of the compound series are presented. The results of the hyphenated TG–MS measurements are evaluated. The limitations of the applied techniques are discussed, too. The principles of here described evaluation steps of the thermoanalytical curves can be generally applied not only to ILs but to most of the sample types. [ABSTRACT FROM AUTHOR]
– Name: AbstractSuppliedCopyright
  Label:
  Group: Ab
  Data: <i>Copyright of Journal of Thermal Analysis & Calorimetry is the property of Springer Nature and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.)
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RecordInfo BibRecord:
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      – Type: doi
        Value: 10.1007/s10973-023-12439-z
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      – Code: eng
        Text: English
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        PageCount: 13
        StartPage: 11407
    Subjects:
      – SubjectFull: Liquid analysis
        Type: general
      – SubjectFull: Ionic liquids
        Type: general
      – SubjectFull: Debye temperatures
        Type: general
      – SubjectFull: Thermal analysis
        Type: general
      – SubjectFull: Data visualization
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      – TitleFull: Tutorial for thermal analysis of ionic liquids.
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            NameFull: Papović, Snežana
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            NameFull: Vraneš, Milan
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            NameFull: Barta Holló, Berta
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            NameFull: Mészáros Szécsényi, Katalin
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            – D: 15
              M: 10
              Text: Oct2024
              Type: published
              Y: 2024
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            – TitleFull: Journal of Thermal Analysis & Calorimetry
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