Improved precision and mechanical properties of 3D‐printed silica ceramics via sintering temperature optimization.

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Title: Improved precision and mechanical properties of 3D‐printed silica ceramics via sintering temperature optimization.
Authors: Mu, Yunsong1,2 (AUTHOR), Chen, Yanhua1,2 (AUTHOR) cyh@xju.edu.cn, Li, He1,2 (AUTHOR) lihe@xju.edu.cn, Sun, Jingwen1,2 (AUTHOR), Mu, Baoxia3 (AUTHOR), Colombo, Paolo4 (AUTHOR)
Source: International Journal of Applied Ceramic Technology. Jan2025, Vol. 22 Issue 1, p1-13. 13p.
Subjects: Precision casting, Turbine blades, Mechanical wear, Flexural strength, Surface roughness
Abstract: Ceramic cores are the key components of precision casting hollow turbine blades, and 3D‐printed silica‐based ceramic cores are crucial to the development of the aerospace industry. However, silica‐based ceramic cores have problems in terms of mechanical properties and friction properties. In this paper, silica ceramics were prepared by stereolithography‐based 3D printing technology and processed at different sintering temperatures. The effect of sintering temperature on the microstructure, physical–mechanical properties, and friction and wear properties of the silica ceramics was investigated. The results show that, with the increase of sintering temperature, the average particle size and bulk density of the samples increased, while the open porosity and layer thickness decreased. The surface of ceramics became more and more flat with the increase in temperature. The flexural strength first increased with increasing temperature, and then suddenly decreased at 1350°C. The average surface roughness decreased with increasing temperature. The wear of the material decreased with increasing sintering temperature and increased at 1350°C. The optimum sintering temperatures were 1250°C and 1300°C, giving a flexural strength of 23.18 and 23.25 MPa, bulk density of 1.72 and 1.78 g/cm3, and open porosity of 24.49% and 23.66%, respectively. [ABSTRACT FROM AUTHOR]
Copyright of International Journal of Applied Ceramic Technology is the property of Wiley-Blackwell and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)
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  Label: Title
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  Data: Improved precision and mechanical properties of 3D‐printed silica ceramics via sintering temperature optimization.
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  Data: <searchLink fieldCode="AR" term="%22Mu%2C+Yunsong%22">Mu, Yunsong</searchLink><relatesTo>1,2</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Chen%2C+Yanhua%22">Chen, Yanhua</searchLink><relatesTo>1,2</relatesTo> (AUTHOR)<i> cyh@xju.edu.cn</i><br /><searchLink fieldCode="AR" term="%22Li%2C+He%22">Li, He</searchLink><relatesTo>1,2</relatesTo> (AUTHOR)<i> lihe@xju.edu.cn</i><br /><searchLink fieldCode="AR" term="%22Sun%2C+Jingwen%22">Sun, Jingwen</searchLink><relatesTo>1,2</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Mu%2C+Baoxia%22">Mu, Baoxia</searchLink><relatesTo>3</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Colombo%2C+Paolo%22">Colombo, Paolo</searchLink><relatesTo>4</relatesTo> (AUTHOR)
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  Data: <searchLink fieldCode="JN" term="%22International+Journal+of+Applied+Ceramic+Technology%22">International Journal of Applied Ceramic Technology</searchLink>. Jan2025, Vol. 22 Issue 1, p1-13. 13p.
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  Data: <searchLink fieldCode="DE" term="%22Precision+casting%22">Precision casting</searchLink><br /><searchLink fieldCode="DE" term="%22Turbine+blades%22">Turbine blades</searchLink><br /><searchLink fieldCode="DE" term="%22Mechanical+wear%22">Mechanical wear</searchLink><br /><searchLink fieldCode="DE" term="%22Flexural+strength%22">Flexural strength</searchLink><br /><searchLink fieldCode="DE" term="%22Surface+roughness%22">Surface roughness</searchLink>
– Name: Abstract
  Label: Abstract
  Group: Ab
  Data: Ceramic cores are the key components of precision casting hollow turbine blades, and 3D‐printed silica‐based ceramic cores are crucial to the development of the aerospace industry. However, silica‐based ceramic cores have problems in terms of mechanical properties and friction properties. In this paper, silica ceramics were prepared by stereolithography‐based 3D printing technology and processed at different sintering temperatures. The effect of sintering temperature on the microstructure, physical–mechanical properties, and friction and wear properties of the silica ceramics was investigated. The results show that, with the increase of sintering temperature, the average particle size and bulk density of the samples increased, while the open porosity and layer thickness decreased. The surface of ceramics became more and more flat with the increase in temperature. The flexural strength first increased with increasing temperature, and then suddenly decreased at 1350°C. The average surface roughness decreased with increasing temperature. The wear of the material decreased with increasing sintering temperature and increased at 1350°C. The optimum sintering temperatures were 1250°C and 1300°C, giving a flexural strength of 23.18 and 23.25 MPa, bulk density of 1.72 and 1.78 g/cm3, and open porosity of 24.49% and 23.66%, respectively. [ABSTRACT FROM AUTHOR]
– Name: AbstractSuppliedCopyright
  Label:
  Group: Ab
  Data: <i>Copyright of International Journal of Applied Ceramic Technology is the property of Wiley-Blackwell and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.)
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RecordInfo BibRecord:
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    Identifiers:
      – Type: doi
        Value: 10.1111/ijac.14880
    Languages:
      – Code: eng
        Text: English
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      Pagination:
        PageCount: 13
        StartPage: 1
    Subjects:
      – SubjectFull: Precision casting
        Type: general
      – SubjectFull: Turbine blades
        Type: general
      – SubjectFull: Mechanical wear
        Type: general
      – SubjectFull: Flexural strength
        Type: general
      – SubjectFull: Surface roughness
        Type: general
    Titles:
      – TitleFull: Improved precision and mechanical properties of 3D‐printed silica ceramics via sintering temperature optimization.
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            NameFull: Mu, Yunsong
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            NameFull: Chen, Yanhua
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            NameFull: Li, He
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            NameFull: Sun, Jingwen
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            NameFull: Mu, Baoxia
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            NameFull: Colombo, Paolo
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            – D: 01
              M: 01
              Text: Jan2025
              Type: published
              Y: 2025
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