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Novel ambient-condition solid-state synthesis route of nanocrystalline TiN thin films via spark plasma ablation deposition.

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Title: Novel ambient-condition solid-state synthesis route of nanocrystalline TiN thin films via spark plasma ablation deposition.
Authors: Radovanović-Perić, Floren1 (AUTHOR) fradovano@fkit.unizg.hr, Burtscher, Michael2 (AUTHOR), Panžić, Ivana1,3 (AUTHOR), Kiener, Daniel2 (AUTHOR), Mandić, Vilko1 (AUTHOR) vmandic@fkit.unizg.hr
Source: Ceramics International. Feb2025, Vol. 51 Issue 5, p5576-5582. 7p.
Subjects: Titanium nitride, Thin film deposition, Plasma deposition, Thin films, Nanoparticle size
Abstract: By utilizing a novel, green and efficient spark plasma ablation deposition, <10 nm size titanium nitride nanoparticles were obtained. The prepared nanopowder material can be utilized for the deposition of a nanocrystalline thin film. The solid-state synthesis was performed completely at ambient conditions, without the use of solvents and post-processing. Transmission electron microscopy confirmed the size of the nanoparticles within the range of less than 10 nm with primary particles as small as 3 nm, while selective area diffraction confirmed fits cubic titanium nitride (TiN) crystal structure. The geometry (thickness and surface roughness) of the deposited thin films could be varied depending on the sparking current and flow rate. Raman spectroscopy suggested the specific morphology that stems from the plastic deformation of nanoparticles upon collision with the substrate might influence the nanolocal structural environment due to a high surface contribution of tensile stress. [ABSTRACT FROM AUTHOR]
Copyright of Ceramics International is the property of Elsevier B.V. and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)
Database: Engineering Source
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Header DbId: egs
DbLabel: Engineering Source
An: 182855070
AccessLevel: 6
PubType: Academic Journal
PubTypeId: academicJournal
PreciseRelevancyScore: 0
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  Data: Novel ambient-condition solid-state synthesis route of nanocrystalline TiN thin films via spark plasma ablation deposition.
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  Data: &lt;searchLink fieldCode=&quot;AR&quot; term=&quot;%22Radovanović-Perić%2C+Floren%22&quot;&gt;Radovanović-Perić, Floren&lt;/searchLink&gt;&lt;relatesTo&gt;1&lt;/relatesTo&gt; (AUTHOR)&lt;i&gt; fradovano@fkit.unizg.hr&lt;/i&gt;&lt;br /&gt;&lt;searchLink fieldCode=&quot;AR&quot; term=&quot;%22Burtscher%2C+Michael%22&quot;&gt;Burtscher, Michael&lt;/searchLink&gt;&lt;relatesTo&gt;2&lt;/relatesTo&gt; (AUTHOR)&lt;br /&gt;&lt;searchLink fieldCode=&quot;AR&quot; term=&quot;%22Panžić%2C+Ivana%22&quot;&gt;Panžić, Ivana&lt;/searchLink&gt;&lt;relatesTo&gt;1,3&lt;/relatesTo&gt; (AUTHOR)&lt;br /&gt;&lt;searchLink fieldCode=&quot;AR&quot; term=&quot;%22Kiener%2C+Daniel%22&quot;&gt;Kiener, Daniel&lt;/searchLink&gt;&lt;relatesTo&gt;2&lt;/relatesTo&gt; (AUTHOR)&lt;br /&gt;&lt;searchLink fieldCode=&quot;AR&quot; term=&quot;%22Mandić%2C+Vilko%22&quot;&gt;Mandić, Vilko&lt;/searchLink&gt;&lt;relatesTo&gt;1&lt;/relatesTo&gt; (AUTHOR)&lt;i&gt; vmandic@fkit.unizg.hr&lt;/i&gt;
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  Data: &lt;searchLink fieldCode=&quot;JN&quot; term=&quot;%22Ceramics+International%22&quot;&gt;Ceramics International&lt;/searchLink&gt;. Feb2025, Vol. 51 Issue 5, p5576-5582. 7p.
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  Data: &lt;searchLink fieldCode=&quot;DE&quot; term=&quot;%22Titanium+nitride%22&quot;&gt;Titanium nitride&lt;/searchLink&gt;&lt;br /&gt;&lt;searchLink fieldCode=&quot;DE&quot; term=&quot;%22Thin+film+deposition%22&quot;&gt;Thin film deposition&lt;/searchLink&gt;&lt;br /&gt;&lt;searchLink fieldCode=&quot;DE&quot; term=&quot;%22Plasma+deposition%22&quot;&gt;Plasma deposition&lt;/searchLink&gt;&lt;br /&gt;&lt;searchLink fieldCode=&quot;DE&quot; term=&quot;%22Thin+films%22&quot;&gt;Thin films&lt;/searchLink&gt;&lt;br /&gt;&lt;searchLink fieldCode=&quot;DE&quot; term=&quot;%22Nanoparticle+size%22&quot;&gt;Nanoparticle size&lt;/searchLink&gt;
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  Data: By utilizing a novel, green and efficient spark plasma ablation deposition, &lt;10 nm size titanium nitride nanoparticles were obtained. The prepared nanopowder material can be utilized for the deposition of a nanocrystalline thin film. The solid-state synthesis was performed completely at ambient conditions, without the use of solvents and post-processing. Transmission electron microscopy confirmed the size of the nanoparticles within the range of less than 10 nm with primary particles as small as 3 nm, while selective area diffraction confirmed fits cubic titanium nitride (TiN) crystal structure. The geometry (thickness and surface roughness) of the deposited thin films could be varied depending on the sparking current and flow rate. Raman spectroscopy suggested the specific morphology that stems from the plastic deformation of nanoparticles upon collision with the substrate might influence the nanolocal structural environment due to a high surface contribution of tensile stress. [ABSTRACT FROM AUTHOR]
– Name: AbstractSuppliedCopyright
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  Data: &lt;i&gt;Copyright of Ceramics International is the property of Elsevier B.V. and its content may not be copied or emailed to multiple sites without the copyright holder&#39;s express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.&lt;/i&gt; (Copyright applies to all Abstracts.)
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      – Type: doi
        Value: 10.1016/j.ceramint.2024.08.028
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      – Code: eng
        Text: English
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        PageCount: 7
        StartPage: 5576
    Subjects:
      – SubjectFull: Titanium nitride
        Type: general
      – SubjectFull: Thin film deposition
        Type: general
      – SubjectFull: Plasma deposition
        Type: general
      – SubjectFull: Thin films
        Type: general
      – SubjectFull: Nanoparticle size
        Type: general
    Titles:
      – TitleFull: Novel ambient-condition solid-state synthesis route of nanocrystalline TiN thin films via spark plasma ablation deposition.
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            NameFull: Radovanović-Perić, Floren
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            NameFull: Burtscher, Michael
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            NameFull: Panžić, Ivana
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            – D: 20
              M: 02
              Text: Feb2025
              Type: published
              Y: 2025
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              Value: 51
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