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Synthesis and Characterization of Variable-Sized Silver Nanoparticles Using Pistacia palaestina Leaf Extract.

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Title: Synthesis and Characterization of Variable-Sized Silver Nanoparticles Using Pistacia palaestina Leaf Extract.
Authors: Musa, Ishaq1 (AUTHOR) i.musa@ptuk.edu.ps, Mousa, Rahaf1 (AUTHOR)
Source: Plasmonics. Mar2025, Vol. 20 Issue 3, p1205-1213. 9p.
Subjects: Scanning probe microscopy, Surface plasmon resonance, Physical & theoretical chemistry, Nanoparticle size, Raman spectroscopy, Silver nitrate
Abstract: Pistacia palaestina (P. palaestina) leaf extract was employed in the synthesis of spherical silver (Ag) nanoparticles, serving as a dual-purpose agent for both reduction and stabilization. These nanoparticles exhibited a range of average sizes between 2 and 27 nm. The size of these nanoparticles was observed to change in response to different concentrations of silver nitrate (AgNO3). This indicates that an increase in AgNO3 concentration leads to a reduction in the size of the nanoparticles. The height and morphology were analyzed using scanning probe microscopy (SPM). The crystalline nature of the Ag nanoparticles was confirmed by XRD analysis. Several properties of Ag nanoparticles, including their Raman spectroscopy, UV–visible absorption, and photoluminescence (PL), have been studied. The Raman spectroscopy revealed prominent peaks at 585 cm−1 assigned to skeletal deformation of C-S-C and 1580 cm−1 is linked to symmetric in plane C − C ring stretching. In the UV–visible spectrophotometry analysis, a surface plasmon resonance (SPR) band was observed, ranging between 395 and 398 nm. Additionally, the photoluminescence properties of these nanoparticles were found to vary with the excitation wavelength, marked by a distinct peak at 365 nm, a shoulder peak at 395 nm, and broader peaks observed at 470, 640, 700, and 740 nm. Furthermore, optical analyses of P. palaestina leaf extract indicated the presence of significant active compounds, including polyphenols, glycerol, and chlorophylls. [ABSTRACT FROM AUTHOR]
Copyright of Plasmonics is the property of Springer Nature and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)
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  Data: Synthesis and Characterization of Variable-Sized Silver Nanoparticles Using Pistacia palaestina Leaf Extract.
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  Data: <searchLink fieldCode="JN" term="%22Plasmonics%22">Plasmonics</searchLink>. Mar2025, Vol. 20 Issue 3, p1205-1213. 9p.
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  Data: <searchLink fieldCode="DE" term="%22Scanning+probe+microscopy%22">Scanning probe microscopy</searchLink><br /><searchLink fieldCode="DE" term="%22Surface+plasmon+resonance%22">Surface plasmon resonance</searchLink><br /><searchLink fieldCode="DE" term="%22Physical+%26+theoretical+chemistry%22">Physical & theoretical chemistry</searchLink><br /><searchLink fieldCode="DE" term="%22Nanoparticle+size%22">Nanoparticle size</searchLink><br /><searchLink fieldCode="DE" term="%22Raman+spectroscopy%22">Raman spectroscopy</searchLink><br /><searchLink fieldCode="DE" term="%22Silver+nitrate%22">Silver nitrate</searchLink>
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  Data: Pistacia palaestina (P. palaestina) leaf extract was employed in the synthesis of spherical silver (Ag) nanoparticles, serving as a dual-purpose agent for both reduction and stabilization. These nanoparticles exhibited a range of average sizes between 2 and 27 nm. The size of these nanoparticles was observed to change in response to different concentrations of silver nitrate (AgNO3). This indicates that an increase in AgNO3 concentration leads to a reduction in the size of the nanoparticles. The height and morphology were analyzed using scanning probe microscopy (SPM). The crystalline nature of the Ag nanoparticles was confirmed by XRD analysis. Several properties of Ag nanoparticles, including their Raman spectroscopy, UV–visible absorption, and photoluminescence (PL), have been studied. The Raman spectroscopy revealed prominent peaks at 585 cm−1 assigned to skeletal deformation of C-S-C and 1580 cm−1 is linked to symmetric in plane C − C ring stretching. In the UV–visible spectrophotometry analysis, a surface plasmon resonance (SPR) band was observed, ranging between 395 and 398 nm. Additionally, the photoluminescence properties of these nanoparticles were found to vary with the excitation wavelength, marked by a distinct peak at 365 nm, a shoulder peak at 395 nm, and broader peaks observed at 470, 640, 700, and 740 nm. Furthermore, optical analyses of P. palaestina leaf extract indicated the presence of significant active compounds, including polyphenols, glycerol, and chlorophylls. [ABSTRACT FROM AUTHOR]
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  Data: <i>Copyright of Plasmonics is the property of Springer Nature and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.)
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        Value: 10.1007/s11468-024-02367-5
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        Text: English
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      – SubjectFull: Surface plasmon resonance
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      – SubjectFull: Physical & theoretical chemistry
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              Text: Mar2025
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