Microstructure and wear resistance of zirconium manufactured by laser directed energy deposition.

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Title: Microstructure and wear resistance of zirconium manufactured by laser directed energy deposition.
Authors: Hu, Chaodan1 (AUTHOR), Chai, Linjiang1 (AUTHOR) chailinjiang@cqut.edu.cn, Wang, Zhichen1 (AUTHOR), Yang, Tao1 (AUTHOR), Tang, Yi1 (AUTHOR), Wang, Zhongwei1 (AUTHOR), Gong, Weijia2 (AUTHOR), Murty, Korukonda L.3 (AUTHOR)
Source: International Journal of Refractory Metals & Hard Materials. Aug2025, Vol. 130, pN.PAG-N.PAG. 1p.
Subjects: Wear resistance, Mechanical wear, Grain refinement, Zirconium, Grain size
Abstract: In this study, a zirconium sheet was fabricated utilizing laser directed energy deposition (L-DED) technique along with its microstructure, hardness, and wear resistance to be compared with a conventionally rolled and annealed (RA) zirconium sheet. The RA specimen exhibits equiaxed grains with uniform size and a bimodal basal texture, along with a few dispersed ZrFe 2 particles. In contrast, the L-DED specimen is featured by parallel or interlaced laths (with dense entangled dislocations) and many Zr 3 Fe precipitates along the lath boundaries, exhibiting a nearly random texture. Tests reveal that the L-DED specimen shows nearly two times hardness and a ∼ 30 % reduced wear rate compared to the RA specimen. Such improvement can be jointly attributed to the enhanced second-phase, dislocation and grain refinement hardening/strengthening. This study verifies the feasibility of producing high performance zirconium materials through L-DED, which could provide some definite insight into further application of additive manufacturing to zirconium production. • Zirconium sheet was fabricated by L-DED and compared with conventionally processed sheet. • L-DED specimen is featured by lath structures with many Zr 3 Fe precipitates along lath boundaries. • L-DED specimen shows nearly doubled hardness and ∼ 30 % reduced wear rate compared to RA specimen. • Such improvement is attributed to enhanced second-phase, dislocation and grain refinement hardening. [ABSTRACT FROM AUTHOR]
Copyright of International Journal of Refractory Metals & Hard Materials is the property of Elsevier B.V. and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)
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Items – Name: Title
  Label: Title
  Group: Ti
  Data: Microstructure and wear resistance of zirconium manufactured by laser directed energy deposition.
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  Data: <searchLink fieldCode="AR" term="%22Hu%2C+Chaodan%22">Hu, Chaodan</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Chai%2C+Linjiang%22">Chai, Linjiang</searchLink><relatesTo>1</relatesTo> (AUTHOR)<i> chailinjiang@cqut.edu.cn</i><br /><searchLink fieldCode="AR" term="%22Wang%2C+Zhichen%22">Wang, Zhichen</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Yang%2C+Tao%22">Yang, Tao</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Tang%2C+Yi%22">Tang, Yi</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Wang%2C+Zhongwei%22">Wang, Zhongwei</searchLink><relatesTo>1</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Gong%2C+Weijia%22">Gong, Weijia</searchLink><relatesTo>2</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Murty%2C+Korukonda+L%2E%22">Murty, Korukonda L.</searchLink><relatesTo>3</relatesTo> (AUTHOR)
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  Data: <searchLink fieldCode="JN" term="%22International+Journal+of+Refractory+Metals+%26+Hard+Materials%22">International Journal of Refractory Metals & Hard Materials</searchLink>. Aug2025, Vol. 130, pN.PAG-N.PAG. 1p.
– Name: Subject
  Label: Subjects
  Group: Su
  Data: <searchLink fieldCode="DE" term="%22Wear+resistance%22">Wear resistance</searchLink><br /><searchLink fieldCode="DE" term="%22Mechanical+wear%22">Mechanical wear</searchLink><br /><searchLink fieldCode="DE" term="%22Grain+refinement%22">Grain refinement</searchLink><br /><searchLink fieldCode="DE" term="%22Zirconium%22">Zirconium</searchLink><br /><searchLink fieldCode="DE" term="%22Grain+size%22">Grain size</searchLink>
– Name: Abstract
  Label: Abstract
  Group: Ab
  Data: In this study, a zirconium sheet was fabricated utilizing laser directed energy deposition (L-DED) technique along with its microstructure, hardness, and wear resistance to be compared with a conventionally rolled and annealed (RA) zirconium sheet. The RA specimen exhibits equiaxed grains with uniform size and a bimodal basal texture, along with a few dispersed ZrFe 2 particles. In contrast, the L-DED specimen is featured by parallel or interlaced laths (with dense entangled dislocations) and many Zr 3 Fe precipitates along the lath boundaries, exhibiting a nearly random texture. Tests reveal that the L-DED specimen shows nearly two times hardness and a ∼ 30 % reduced wear rate compared to the RA specimen. Such improvement can be jointly attributed to the enhanced second-phase, dislocation and grain refinement hardening/strengthening. This study verifies the feasibility of producing high performance zirconium materials through L-DED, which could provide some definite insight into further application of additive manufacturing to zirconium production. • Zirconium sheet was fabricated by L-DED and compared with conventionally processed sheet. • L-DED specimen is featured by lath structures with many Zr 3 Fe precipitates along lath boundaries. • L-DED specimen shows nearly doubled hardness and ∼ 30 % reduced wear rate compared to RA specimen. • Such improvement is attributed to enhanced second-phase, dislocation and grain refinement hardening. [ABSTRACT FROM AUTHOR]
– Name: AbstractSuppliedCopyright
  Label:
  Group: Ab
  Data: <i>Copyright of International Journal of Refractory Metals & Hard Materials is the property of Elsevier B.V. and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.)
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RecordInfo BibRecord:
  BibEntity:
    Identifiers:
      – Type: doi
        Value: 10.1016/j.ijrmhm.2025.107168
    Languages:
      – Code: eng
        Text: English
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      Pagination:
        PageCount: 1
        StartPage: N.PAG
    Subjects:
      – SubjectFull: Wear resistance
        Type: general
      – SubjectFull: Mechanical wear
        Type: general
      – SubjectFull: Grain refinement
        Type: general
      – SubjectFull: Zirconium
        Type: general
      – SubjectFull: Grain size
        Type: general
    Titles:
      – TitleFull: Microstructure and wear resistance of zirconium manufactured by laser directed energy deposition.
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            NameFull: Hu, Chaodan
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            NameFull: Chai, Linjiang
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            NameFull: Wang, Zhichen
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            NameFull: Yang, Tao
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            NameFull: Tang, Yi
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            NameFull: Wang, Zhongwei
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            NameFull: Gong, Weijia
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            NameFull: Murty, Korukonda L.
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          Dates:
            – D: 01
              M: 08
              Text: Aug2025
              Type: published
              Y: 2025
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              Value: 130
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            – TitleFull: International Journal of Refractory Metals & Hard Materials
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