View in EDS HTML Full Text PDF Full Text

Densification of hard β‐boron based ceramics by spark plasma sintering at larger heating rate.

Saved in:
Bibliographic Details
Title: Densification of hard β‐boron based ceramics by spark plasma sintering at larger heating rate.
Authors: Xiong, Zhengang1,2 (AUTHOR), Zou, Ji1,2 (AUTHOR) ji.zou@whut.edu.cn, Ma, Haibin3 (AUTHOR), Ji, Wei1,2 (AUTHOR), Wang, Weimin1,2 (AUTHOR), Fu, Zhengyi1,2 (AUTHOR)
Source: Journal of the American Ceramic Society. Sep2025, Vol. 108 Issue 9, p1-9. 9p.
Subjects: Vickers hardness, Thermal plasmas, Thermal properties, Boron, Porosity
Abstract: The densification process of β‐boron via spark plasma sintering (SPS) with controlled heating rates (50–300°C/min) was investigated at different temperatures from 1000°C to 1800°C. Systematic characterization reveals that enhanced heating rates (300°C/min) effectively suppress the volatilization of B2O3 impurities, promoting in situ formation of boron‐rich oxide (B6O) through reactions between boron and B2O3. The amount of the retained B6O phase in the boron matrix increased with heating rates, which effectively accelerate the densification behavior of boron , achieving near‐full density (2.33 g/cm3) with residual porosity < 0.3% in consolidated boron ceramics. Resultant ceramics demonstrate good combination of properties, including high Vickers hardness (31.0 ± 1.8 GPa at 9.8 N) and low thermal conductivity (13.8 W·m−1·K−1 at room temperature and 5.8 W·m−1·K−1 at 873 K), the latter was governed by intensified phonon–phonon scattering with less contributions from electrons (< 1‰). [ABSTRACT FROM AUTHOR]
Copyright of Journal of the American Ceramic Society is the property of Wiley-Blackwell and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)
Database: Engineering Source
Full text is not displayed to guests.
FullText Links:
  – Type: pdflink
Text:
  Availability: 1
Header DbId: egs
DbLabel: Engineering Source
An: 186371228
AccessLevel: 6
PubType: Academic Journal
PubTypeId: academicJournal
PreciseRelevancyScore: 0
IllustrationInfo
Items – Name: Title
  Label: Title
  Group: Ti
  Data: Densification of hard β‐boron based ceramics by spark plasma sintering at larger heating rate.
– Name: Author
  Label: Authors
  Group: Au
  Data: &lt;searchLink fieldCode=&quot;AR&quot; term=&quot;%22Xiong%2C+Zhengang%22&quot;&gt;Xiong, Zhengang&lt;/searchLink&gt;&lt;relatesTo&gt;1,2&lt;/relatesTo&gt; (AUTHOR)&lt;br /&gt;&lt;searchLink fieldCode=&quot;AR&quot; term=&quot;%22Zou%2C+Ji%22&quot;&gt;Zou, Ji&lt;/searchLink&gt;&lt;relatesTo&gt;1,2&lt;/relatesTo&gt; (AUTHOR)&lt;i&gt; ji.zou@whut.edu.cn&lt;/i&gt;&lt;br /&gt;&lt;searchLink fieldCode=&quot;AR&quot; term=&quot;%22Ma%2C+Haibin%22&quot;&gt;Ma, Haibin&lt;/searchLink&gt;&lt;relatesTo&gt;3&lt;/relatesTo&gt; (AUTHOR)&lt;br /&gt;&lt;searchLink fieldCode=&quot;AR&quot; term=&quot;%22Ji%2C+Wei%22&quot;&gt;Ji, Wei&lt;/searchLink&gt;&lt;relatesTo&gt;1,2&lt;/relatesTo&gt; (AUTHOR)&lt;br /&gt;&lt;searchLink fieldCode=&quot;AR&quot; term=&quot;%22Wang%2C+Weimin%22&quot;&gt;Wang, Weimin&lt;/searchLink&gt;&lt;relatesTo&gt;1,2&lt;/relatesTo&gt; (AUTHOR)&lt;br /&gt;&lt;searchLink fieldCode=&quot;AR&quot; term=&quot;%22Fu%2C+Zhengyi%22&quot;&gt;Fu, Zhengyi&lt;/searchLink&gt;&lt;relatesTo&gt;1,2&lt;/relatesTo&gt; (AUTHOR)
– Name: TitleSource
  Label: Source
  Group: Src
  Data: &lt;searchLink fieldCode=&quot;JN&quot; term=&quot;%22Journal+of+the+American+Ceramic+Society%22&quot;&gt;Journal of the American Ceramic Society&lt;/searchLink&gt;. Sep2025, Vol. 108 Issue 9, p1-9. 9p.
– Name: Subject
  Label: Subjects
  Group: Su
  Data: &lt;searchLink fieldCode=&quot;DE&quot; term=&quot;%22Vickers+hardness%22&quot;&gt;Vickers hardness&lt;/searchLink&gt;&lt;br /&gt;&lt;searchLink fieldCode=&quot;DE&quot; term=&quot;%22Thermal+plasmas%22&quot;&gt;Thermal plasmas&lt;/searchLink&gt;&lt;br /&gt;&lt;searchLink fieldCode=&quot;DE&quot; term=&quot;%22Thermal+properties%22&quot;&gt;Thermal properties&lt;/searchLink&gt;&lt;br /&gt;&lt;searchLink fieldCode=&quot;DE&quot; term=&quot;%22Boron%22&quot;&gt;Boron&lt;/searchLink&gt;&lt;br /&gt;&lt;searchLink fieldCode=&quot;DE&quot; term=&quot;%22Porosity%22&quot;&gt;Porosity&lt;/searchLink&gt;
– Name: Abstract
  Label: Abstract
  Group: Ab
  Data: The densification process of β‐boron via spark plasma sintering (SPS) with controlled heating rates (50–300&#176;C/min) was investigated at different temperatures from 1000&#176;C to 1800&#176;C. Systematic characterization reveals that enhanced heating rates (300&#176;C/min) effectively suppress the volatilization of B2O3 impurities, promoting in situ formation of boron‐rich oxide (B6O) through reactions between boron and B2O3. The amount of the retained B6O phase in the boron matrix increased with heating rates, which effectively accelerate the densification behavior of boron , achieving near‐full density (2.33 g/cm3) with residual porosity &lt; 0.3% in consolidated boron ceramics. Resultant ceramics demonstrate good combination of properties, including high Vickers hardness (31.0 &#177; 1.8 GPa at 9.8 N) and low thermal conductivity (13.8 W&#183;m−1&#183;K−1 at room temperature and 5.8 W&#183;m−1&#183;K−1 at 873 K), the latter was governed by intensified phonon–phonon scattering with less contributions from electrons (&lt; 1‰). [ABSTRACT FROM AUTHOR]
– Name: AbstractSuppliedCopyright
  Label:
  Group: Ab
  Data: &lt;i&gt;Copyright of Journal of the American Ceramic Society is the property of Wiley-Blackwell and its content may not be copied or emailed to multiple sites without the copyright holder&#39;s express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.&lt;/i&gt; (Copyright applies to all Abstracts.)
PLink https://search.ebscohost.com/login.aspx?direct=true&site=eds-live&db=egs&AN=186371228
RecordInfo BibRecord:
  BibEntity:
    Identifiers:
      – Type: doi
        Value: 10.1111/jace.20679
    Languages:
      – Code: eng
        Text: English
    PhysicalDescription:
      Pagination:
        PageCount: 9
        StartPage: 1
    Subjects:
      – SubjectFull: Vickers hardness
        Type: general
      – SubjectFull: Thermal plasmas
        Type: general
      – SubjectFull: Thermal properties
        Type: general
      – SubjectFull: Boron
        Type: general
      – SubjectFull: Porosity
        Type: general
    Titles:
      – TitleFull: Densification of hard β‐boron based ceramics by spark plasma sintering at larger heating rate.
        Type: main
  BibRelationships:
    HasContributorRelationships:
      – PersonEntity:
          Name:
            NameFull: Xiong, Zhengang
      – PersonEntity:
          Name:
            NameFull: Zou, Ji
      – PersonEntity:
          Name:
            NameFull: Ma, Haibin
      – PersonEntity:
          Name:
            NameFull: Ji, Wei
      – PersonEntity:
          Name:
            NameFull: Wang, Weimin
      – PersonEntity:
          Name:
            NameFull: Fu, Zhengyi
    IsPartOfRelationships:
      – BibEntity:
          Dates:
            – D: 01
              M: 09
              Text: Sep2025
              Type: published
              Y: 2025
          Identifiers:
            – Type: issn-print
              Value: 00027820
          Numbering:
            – Type: volume
              Value: 108
            – Type: issue
              Value: 9
          Titles:
            – TitleFull: Journal of the American Ceramic Society
              Type: main
ResultId 1