The Effect of Strain Aging on the Microstructure and Mechanical Properties of Steel for Reel-Lay Coiled Steel Pipelines.

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Title: The Effect of Strain Aging on the Microstructure and Mechanical Properties of Steel for Reel-Lay Coiled Steel Pipelines.
Authors: Cao, Yuxi1,2 (AUTHOR), Zuo, Guofeng2,3 (AUTHOR), Peng, Yang3 (AUTHOR), Zhu, Lin1,3 (AUTHOR), Tong, Shuai2 (AUTHOR), Yin, Shubiao1,3 (AUTHOR), Sun, Xinjun2 (AUTHOR)
Source: Materials (1996-1944). Aug2025, Vol. 18 Issue 15, p3462. 17p.
Subjects: Microstructure, Dislocation density, Strain hardening, Material plasticity, Mechanical behavior of materials, Steel pipe
Abstract: Deep-sea oil and gas pipelines undergo significant plastic strain during reel-lay installation. Additionally, the static strain aging phenomenon that occurs during service can further deteriorate the mechanical properties of the pipelines. This study investigates the plastic deformation mechanism of reel-lay pipeline steel by subjecting the test steel to 5% pre-strain followed by aging treatment at 250 °C for 1 h. The present study systematically correlates the evolution of mechanical properties with microstructural changes through microstructural characterization techniques such as EBSD, TEM, and XRD. The results demonstrate that after pre-straining, the yield strength of the experimental steel increases due to dislocation strengthening and residual stress generation, while its uniform elongation decreases. Although no significant changes in grain size are observed macroscopically, microstructural characterization reveals a substantial increase in dislocation density within the matrix, forming dislocation cells and walls. These substructures lead to a deterioration of the material's work hardening capacity. Following aging treatment, the tested steel exhibits further increased yield strength and reduced uniform elongation. After aging treatment, although the dislocation density in the matrix slightly decreases and dislocation tangles are somewhat reduced, the Cottrell atmosphere pinning effect leads to a further decline in work hardening capability, ultimately resulting in the deterioration of plasticity in reel-lay pipeline steel. The instantaneous hardening exponent curve shows that the work hardening phenomenon becomes more pronounced in the tested steel after strain aging as the tempering temperature increases. [ABSTRACT FROM AUTHOR]
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  Label: Title
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  Data: The Effect of Strain Aging on the Microstructure and Mechanical Properties of Steel for Reel-Lay Coiled Steel Pipelines.
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  Data: <searchLink fieldCode="JN" term="%22Materials+%281996-1944%29%22">Materials (1996-1944)</searchLink>. Aug2025, Vol. 18 Issue 15, p3462. 17p.
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  Data: <searchLink fieldCode="DE" term="%22Microstructure%22">Microstructure</searchLink><br /><searchLink fieldCode="DE" term="%22Dislocation+density%22">Dislocation density</searchLink><br /><searchLink fieldCode="DE" term="%22Strain+hardening%22">Strain hardening</searchLink><br /><searchLink fieldCode="DE" term="%22Material+plasticity%22">Material plasticity</searchLink><br /><searchLink fieldCode="DE" term="%22Mechanical+behavior+of+materials%22">Mechanical behavior of materials</searchLink><br /><searchLink fieldCode="DE" term="%22Steel+pipe%22">Steel pipe</searchLink>
– Name: Abstract
  Label: Abstract
  Group: Ab
  Data: Deep-sea oil and gas pipelines undergo significant plastic strain during reel-lay installation. Additionally, the static strain aging phenomenon that occurs during service can further deteriorate the mechanical properties of the pipelines. This study investigates the plastic deformation mechanism of reel-lay pipeline steel by subjecting the test steel to 5% pre-strain followed by aging treatment at 250 °C for 1 h. The present study systematically correlates the evolution of mechanical properties with microstructural changes through microstructural characterization techniques such as EBSD, TEM, and XRD. The results demonstrate that after pre-straining, the yield strength of the experimental steel increases due to dislocation strengthening and residual stress generation, while its uniform elongation decreases. Although no significant changes in grain size are observed macroscopically, microstructural characterization reveals a substantial increase in dislocation density within the matrix, forming dislocation cells and walls. These substructures lead to a deterioration of the material's work hardening capacity. Following aging treatment, the tested steel exhibits further increased yield strength and reduced uniform elongation. After aging treatment, although the dislocation density in the matrix slightly decreases and dislocation tangles are somewhat reduced, the Cottrell atmosphere pinning effect leads to a further decline in work hardening capability, ultimately resulting in the deterioration of plasticity in reel-lay pipeline steel. The instantaneous hardening exponent curve shows that the work hardening phenomenon becomes more pronounced in the tested steel after strain aging as the tempering temperature increases. [ABSTRACT FROM AUTHOR]
– Name: AbstractSuppliedCopyright
  Label:
  Group: Ab
  Data: <i>Copyright of Materials (1996-1944) is the property of MDPI and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.)
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        Value: 10.3390/ma18153462
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        Text: English
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        PageCount: 17
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      – SubjectFull: Microstructure
        Type: general
      – SubjectFull: Dislocation density
        Type: general
      – SubjectFull: Strain hardening
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      – SubjectFull: Material plasticity
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      – SubjectFull: Mechanical behavior of materials
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      – SubjectFull: Steel pipe
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      – TitleFull: The Effect of Strain Aging on the Microstructure and Mechanical Properties of Steel for Reel-Lay Coiled Steel Pipelines.
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              M: 08
              Text: Aug2025
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              Y: 2025
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