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Twin‐compartment solid–liquid cells for neutron reflectometry.

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Title: Twin‐compartment solid–liquid cells for neutron reflectometry.
Authors: Paracini, Nicoló1,2 (AUTHOR) nicolo.paracini@sund.ku.dk, Burrall, Hannah3 (AUTHOR), Saerbeck, Thomas4 (AUTHOR), Gutfreund, Philipp4 (AUTHOR), Fragneto, Giovanna3 (AUTHOR), Clifton, Luke A.5 (AUTHOR), Arnold, Thomas3 (AUTHOR), Cárdenas, Marité6,7,8 (AUTHOR)
Source: Journal of Applied Crystallography. Apr2026, Vol. 59 Issue 2, p369-380. 12p.
Subjects: Neutron reflectometry, Solid-liquid interfaces, Spin coating, Langmuir-Blodgett films, Sputter deposition, Scientific apparatus & instruments, Substrates (Materials science)
Abstract: We propose a new type of sample environment for neutron reflectometry at solid–liquid interfaces. The twin‐compartment solid–liquid cell optimizes several aspects of neutron reflectometry measurements by splitting the surface of substrates currently in use at facilities into two independent samples. This approach increases the capacity of mounted samples on the stage of current neutron reflectometers by a factor of two, shortens alignment times, and enables side‐by‐side comparison and control experiments on identical substrates. Furthermore, it reduces sample preparation time for a variety of samples prepared by Langmuir monolayer transfer techniques, spin coating, sputter coating, ex situ self‐assembly and more. We present results from three cell prototypes tested on vertical and horizontal reflectometers at ISIS and Institut Laue–Langevin. [ABSTRACT FROM AUTHOR]
Copyright of Journal of Applied Crystallography is the property of Wiley-Blackwell and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)
Database: Engineering Source
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Header DbId: egs
DbLabel: Engineering Source
An: 192849679
AccessLevel: 6
PubType: Academic Journal
PubTypeId: academicJournal
PreciseRelevancyScore: 0
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  Data: Twin‐compartment solid–liquid cells for neutron reflectometry.
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  Data: <searchLink fieldCode="AR" term="%22Paracini%2C+Nicoló%22">Paracini, Nicoló</searchLink><relatesTo>1,2</relatesTo> (AUTHOR)<i> nicolo.paracini@sund.ku.dk</i><br /><searchLink fieldCode="AR" term="%22Burrall%2C+Hannah%22">Burrall, Hannah</searchLink><relatesTo>3</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Saerbeck%2C+Thomas%22">Saerbeck, Thomas</searchLink><relatesTo>4</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Gutfreund%2C+Philipp%22">Gutfreund, Philipp</searchLink><relatesTo>4</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Fragneto%2C+Giovanna%22">Fragneto, Giovanna</searchLink><relatesTo>3</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Clifton%2C+Luke+A%2E%22">Clifton, Luke A.</searchLink><relatesTo>5</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Arnold%2C+Thomas%22">Arnold, Thomas</searchLink><relatesTo>3</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Cárdenas%2C+Marité%22">Cárdenas, Marité</searchLink><relatesTo>6,7,8</relatesTo> (AUTHOR)
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  Data: <searchLink fieldCode="JN" term="%22Journal+of+Applied+Crystallography%22">Journal of Applied Crystallography</searchLink>. Apr2026, Vol. 59 Issue 2, p369-380. 12p.
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  Data: <searchLink fieldCode="DE" term="%22Neutron+reflectometry%22">Neutron reflectometry</searchLink><br /><searchLink fieldCode="DE" term="%22Solid-liquid+interfaces%22">Solid-liquid interfaces</searchLink><br /><searchLink fieldCode="DE" term="%22Spin+coating%22">Spin coating</searchLink><br /><searchLink fieldCode="DE" term="%22Langmuir-Blodgett+films%22">Langmuir-Blodgett films</searchLink><br /><searchLink fieldCode="DE" term="%22Sputter+deposition%22">Sputter deposition</searchLink><br /><searchLink fieldCode="DE" term="%22Scientific+apparatus+%26+instruments%22">Scientific apparatus & instruments</searchLink><br /><searchLink fieldCode="DE" term="%22Substrates+%28Materials+science%29%22">Substrates (Materials science)</searchLink>
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  Data: We propose a new type of sample environment for neutron reflectometry at solid–liquid interfaces. The twin‐compartment solid–liquid cell optimizes several aspects of neutron reflectometry measurements by splitting the surface of substrates currently in use at facilities into two independent samples. This approach increases the capacity of mounted samples on the stage of current neutron reflectometers by a factor of two, shortens alignment times, and enables side‐by‐side comparison and control experiments on identical substrates. Furthermore, it reduces sample preparation time for a variety of samples prepared by Langmuir monolayer transfer techniques, spin coating, sputter coating, ex situ self‐assembly and more. We present results from three cell prototypes tested on vertical and horizontal reflectometers at ISIS and Institut Laue–Langevin. [ABSTRACT FROM AUTHOR]
– Name: AbstractSuppliedCopyright
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  Data: <i>Copyright of Journal of Applied Crystallography is the property of Wiley-Blackwell and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.)
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      – Type: doi
        Value: 10.1107/S1600576726000919
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      – Code: eng
        Text: English
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        PageCount: 12
        StartPage: 369
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      – SubjectFull: Neutron reflectometry
        Type: general
      – SubjectFull: Solid-liquid interfaces
        Type: general
      – SubjectFull: Spin coating
        Type: general
      – SubjectFull: Langmuir-Blodgett films
        Type: general
      – SubjectFull: Sputter deposition
        Type: general
      – SubjectFull: Scientific apparatus & instruments
        Type: general
      – SubjectFull: Substrates (Materials science)
        Type: general
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      – TitleFull: Twin‐compartment solid–liquid cells for neutron reflectometry.
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            – D: 01
              M: 04
              Text: Apr2026
              Type: published
              Y: 2026
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              Value: 00218898
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              Value: 59
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