Effect of Directional Solidification on Microstructural Evolution and Properties of GH3625 Alloy.

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Title: Effect of Directional Solidification on Microstructural Evolution and Properties of GH3625 Alloy.
Authors: Zhang, Yanqin1,2 (AUTHOR), Jia, Zhi1,2 (AUTHOR) jiazhi@lut.edu.cn, Liu, Yafei1,2 (AUTHOR)
Source: Materials (1996-1944). Apr2026, Vol. 19 Issue 7, p1442. 23p.
Subjects: Directional solidification, Microstructure, Mechanical behavior of materials, Corrosion resistance, Nickel alloys, Laves phases (Metallurgy)
Abstract: Nickel-based superalloy GH3625 is widely used in extreme environments due to its exceptional high-temperature strength and corrosion resistance; however, optimizing its comprehensive performance through precise microstructural control remains a critical challenge. In this study, the effect of withdrawal rate (10–200 μm/s) on the microstructural evolution, mechanical properties, and corrosion resistance of GH3625 alloy was investigated using a liquid-metal-cooled directional solidification system. The microstructural characteristics, elemental segregation, and phase distributions were systematically analyzed via OM, SEM, and EDS, followed by uniaxial tensile and electrochemical polarization tests. The results show that with increasing withdrawal rate, the solid–liquid interface morphology evolves from cellular to cellular-dendritic and finally to fully dendritic. Correspondingly, the primary dendrite arm spacing decreases from 270.4 μm to 100.2 μm, and the secondary dendrite arm spacing decreases from 66.5 μm to 12.3 μm. The area fraction of the detrimental Laves phase first decreases and then increases, reaching a minimum at 100 μm/s. Correspondingly, the yield strength increases from 282 MPa to 409 MPa, and the corrosion resistance is optimized at 100 μm/s. The microstructure–property relationships are discussed based on second-phase strengthening theory and microstructural refinement. This study provides a theoretical basis and practical process windows for optimizing directional solidification parameters to achieve enhanced mechanical and corrosion performance in GH3625 alloy. [ABSTRACT FROM AUTHOR]
Copyright of Materials (1996-1944) is the property of MDPI and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)
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  Data: Effect of Directional Solidification on Microstructural Evolution and Properties of GH3625 Alloy.
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  Data: <searchLink fieldCode="AR" term="%22Zhang%2C+Yanqin%22">Zhang, Yanqin</searchLink><relatesTo>1,2</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Jia%2C+Zhi%22">Jia, Zhi</searchLink><relatesTo>1,2</relatesTo> (AUTHOR)<i> jiazhi@lut.edu.cn</i><br /><searchLink fieldCode="AR" term="%22Liu%2C+Yafei%22">Liu, Yafei</searchLink><relatesTo>1,2</relatesTo> (AUTHOR)
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  Data: <searchLink fieldCode="JN" term="%22Materials+%281996-1944%29%22">Materials (1996-1944)</searchLink>. Apr2026, Vol. 19 Issue 7, p1442. 23p.
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  Data: <searchLink fieldCode="DE" term="%22Directional+solidification%22">Directional solidification</searchLink><br /><searchLink fieldCode="DE" term="%22Microstructure%22">Microstructure</searchLink><br /><searchLink fieldCode="DE" term="%22Mechanical+behavior+of+materials%22">Mechanical behavior of materials</searchLink><br /><searchLink fieldCode="DE" term="%22Corrosion+resistance%22">Corrosion resistance</searchLink><br /><searchLink fieldCode="DE" term="%22Nickel+alloys%22">Nickel alloys</searchLink><br /><searchLink fieldCode="DE" term="%22Laves+phases+%28Metallurgy%29%22">Laves phases (Metallurgy)</searchLink>
– Name: Abstract
  Label: Abstract
  Group: Ab
  Data: Nickel-based superalloy GH3625 is widely used in extreme environments due to its exceptional high-temperature strength and corrosion resistance; however, optimizing its comprehensive performance through precise microstructural control remains a critical challenge. In this study, the effect of withdrawal rate (10–200 μm/s) on the microstructural evolution, mechanical properties, and corrosion resistance of GH3625 alloy was investigated using a liquid-metal-cooled directional solidification system. The microstructural characteristics, elemental segregation, and phase distributions were systematically analyzed via OM, SEM, and EDS, followed by uniaxial tensile and electrochemical polarization tests. The results show that with increasing withdrawal rate, the solid–liquid interface morphology evolves from cellular to cellular-dendritic and finally to fully dendritic. Correspondingly, the primary dendrite arm spacing decreases from 270.4 μm to 100.2 μm, and the secondary dendrite arm spacing decreases from 66.5 μm to 12.3 μm. The area fraction of the detrimental Laves phase first decreases and then increases, reaching a minimum at 100 μm/s. Correspondingly, the yield strength increases from 282 MPa to 409 MPa, and the corrosion resistance is optimized at 100 μm/s. The microstructure–property relationships are discussed based on second-phase strengthening theory and microstructural refinement. This study provides a theoretical basis and practical process windows for optimizing directional solidification parameters to achieve enhanced mechanical and corrosion performance in GH3625 alloy. [ABSTRACT FROM AUTHOR]
– Name: AbstractSuppliedCopyright
  Label:
  Group: Ab
  Data: <i>Copyright of Materials (1996-1944) is the property of MDPI and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.)
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        Value: 10.3390/ma19071442
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        Text: English
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        Type: general
      – SubjectFull: Microstructure
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      – SubjectFull: Mechanical behavior of materials
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      – SubjectFull: Corrosion resistance
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      – SubjectFull: Nickel alloys
        Type: general
      – SubjectFull: Laves phases (Metallurgy)
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      – TitleFull: Effect of Directional Solidification on Microstructural Evolution and Properties of GH3625 Alloy.
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            NameFull: Zhang, Yanqin
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            – D: 01
              M: 04
              Text: Apr2026
              Type: published
              Y: 2026
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