Effects of Heat Treatment Procedures and Diamond Burnishing on Tensile Properties and Surface Integrity of Additively Manufactured 17-4PH Steel Cylindrical Parts.

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Title: Effects of Heat Treatment Procedures and Diamond Burnishing on Tensile Properties and Surface Integrity of Additively Manufactured 17-4PH Steel Cylindrical Parts.
Authors: Duncheva, Galya1,2 (AUTHOR) duncheva@tugab.bg, Maximov, Jordan1,2 (AUTHOR), Dunchev, Vladimir1,2,3 (AUTHOR), Anchev, Angel1,2,4 (AUTHOR), Todorov, Vladimir1,2 (AUTHOR), Argirov, Yaroslav2,3 (AUTHOR), Anastasov, Kalin2,3,4 (AUTHOR), Mitev, Hristian2,4 (AUTHOR)
Source: Materials (1996-1944). Jun2026, Vol. 19 Issue 11, p2192. 33p.
Subjects: Heat treatment, Powder bed fusion, Heat treatment of steel, Three-dimensional printing, Surface finishing, Mechanical behavior of materials, Tensile strength, Surface properties
Abstract: This article presents a new combined post-processing concept to improve the quality of laser powder bed fusion (LPBF) of 17-4PH stainless steel (SS) cylindrical parts fabricated from N2-atomised LaserForm 17-4PH (B) powder. The concept is based on consecutive heat treatment procedures and diamond burnishing (DB) processes. A two-stage study was conducted. The first stage was an LPBF process experiment. The following combination of LPBF parameter values was selected after optimisation: a laser power of P = 150   W , laser scanning speed of v = 1200 mm/s, and layer thickness of t = 40   μ m . In the second stage, this combination was used to evaluate the effects of two heat treatment procedures (HT1 and HT2) and two DB processes (using burnishing forces of 100 N and 300 N) on the tensile properties and surface integrity of LPBF 17-4PH SS cylindrical samples. The HT2 procedure, including annealing (1200 ∘ , 4   h) , solution treatment ( 1060 ∘ , 1   h) , cooling ( − 70   ∘ C , 2   h ), and ageing ( 482 ∘ , 4   h ) led to yield limit, tensile strength, and Vickers hardness values of Y L = 1071   M P a , T S = 1410   M P a , and 523   H V , respectively. The concept presented takes advantage of the combination of the transformation, precipitation and strain-hardening effects. The combined effect was most pronounced in the samples subjected to the HT2 procedure and subsequent DB (300 N), for which a retained austenite fraction of 6.93%, surface microhardness of 563   H V 0.05 and the maximum values of the compressive axial and hoop RSs of − 1426.3   M P a and − 1095.9   M P a , respectively, were measured. [ABSTRACT FROM AUTHOR]
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  Label: Title
  Group: Ti
  Data: Effects of Heat Treatment Procedures and Diamond Burnishing on Tensile Properties and Surface Integrity of Additively Manufactured 17-4PH Steel Cylindrical Parts.
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  Data: <searchLink fieldCode="AR" term="%22Duncheva%2C+Galya%22">Duncheva, Galya</searchLink><relatesTo>1,2</relatesTo> (AUTHOR)<i> duncheva@tugab.bg</i><br /><searchLink fieldCode="AR" term="%22Maximov%2C+Jordan%22">Maximov, Jordan</searchLink><relatesTo>1,2</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Dunchev%2C+Vladimir%22">Dunchev, Vladimir</searchLink><relatesTo>1,2,3</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Anchev%2C+Angel%22">Anchev, Angel</searchLink><relatesTo>1,2,4</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Todorov%2C+Vladimir%22">Todorov, Vladimir</searchLink><relatesTo>1,2</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Argirov%2C+Yaroslav%22">Argirov, Yaroslav</searchLink><relatesTo>2,3</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Anastasov%2C+Kalin%22">Anastasov, Kalin</searchLink><relatesTo>2,3,4</relatesTo> (AUTHOR)<br /><searchLink fieldCode="AR" term="%22Mitev%2C+Hristian%22">Mitev, Hristian</searchLink><relatesTo>2,4</relatesTo> (AUTHOR)
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  Data: <searchLink fieldCode="JN" term="%22Materials+%281996-1944%29%22">Materials (1996-1944)</searchLink>. Jun2026, Vol. 19 Issue 11, p2192. 33p.
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  Data: <searchLink fieldCode="DE" term="%22Heat+treatment%22">Heat treatment</searchLink><br /><searchLink fieldCode="DE" term="%22Powder+bed+fusion%22">Powder bed fusion</searchLink><br /><searchLink fieldCode="DE" term="%22Heat+treatment+of+steel%22">Heat treatment of steel</searchLink><br /><searchLink fieldCode="DE" term="%22Three-dimensional+printing%22">Three-dimensional printing</searchLink><br /><searchLink fieldCode="DE" term="%22Surface+finishing%22">Surface finishing</searchLink><br /><searchLink fieldCode="DE" term="%22Mechanical+behavior+of+materials%22">Mechanical behavior of materials</searchLink><br /><searchLink fieldCode="DE" term="%22Tensile+strength%22">Tensile strength</searchLink><br /><searchLink fieldCode="DE" term="%22Surface+properties%22">Surface properties</searchLink>
– Name: Abstract
  Label: Abstract
  Group: Ab
  Data: This article presents a new combined post-processing concept to improve the quality of laser powder bed fusion (LPBF) of 17-4PH stainless steel (SS) cylindrical parts fabricated from N2-atomised LaserForm 17-4PH (B) powder. The concept is based on consecutive heat treatment procedures and diamond burnishing (DB) processes. A two-stage study was conducted. The first stage was an LPBF process experiment. The following combination of LPBF parameter values was selected after optimisation: a laser power of P = 150   W , laser scanning speed of v = 1200 mm/s, and layer thickness of t = 40   μ m . In the second stage, this combination was used to evaluate the effects of two heat treatment procedures (HT1 and HT2) and two DB processes (using burnishing forces of 100 N and 300 N) on the tensile properties and surface integrity of LPBF 17-4PH SS cylindrical samples. The HT2 procedure, including annealing (1200 ∘ , 4   h) , solution treatment ( 1060 ∘ , 1   h) , cooling ( − 70   ∘ C , 2   h ), and ageing ( 482 ∘ , 4   h ) led to yield limit, tensile strength, and Vickers hardness values of Y L = 1071   M P a , T S = 1410   M P a , and 523   H V , respectively. The concept presented takes advantage of the combination of the transformation, precipitation and strain-hardening effects. The combined effect was most pronounced in the samples subjected to the HT2 procedure and subsequent DB (300 N), for which a retained austenite fraction of 6.93%, surface microhardness of 563   H V 0.05 and the maximum values of the compressive axial and hoop RSs of − 1426.3   M P a and − 1095.9   M P a , respectively, were measured. [ABSTRACT FROM AUTHOR]
– Name: AbstractSuppliedCopyright
  Label:
  Group: Ab
  Data: <i>Copyright of Materials (1996-1944) is the property of MDPI and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.)
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      – Type: doi
        Value: 10.3390/ma19112192
    Languages:
      – Code: eng
        Text: English
    PhysicalDescription:
      Pagination:
        PageCount: 33
        StartPage: 2192
    Subjects:
      – SubjectFull: Heat treatment
        Type: general
      – SubjectFull: Powder bed fusion
        Type: general
      – SubjectFull: Heat treatment of steel
        Type: general
      – SubjectFull: Three-dimensional printing
        Type: general
      – SubjectFull: Surface finishing
        Type: general
      – SubjectFull: Mechanical behavior of materials
        Type: general
      – SubjectFull: Tensile strength
        Type: general
      – SubjectFull: Surface properties
        Type: general
    Titles:
      – TitleFull: Effects of Heat Treatment Procedures and Diamond Burnishing on Tensile Properties and Surface Integrity of Additively Manufactured 17-4PH Steel Cylindrical Parts.
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            NameFull: Duncheva, Galya
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            NameFull: Maximov, Jordan
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            NameFull: Dunchev, Vladimir
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            NameFull: Argirov, Yaroslav
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            NameFull: Anastasov, Kalin
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            NameFull: Mitev, Hristian
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            – D: 01
              M: 06
              Text: Jun2026
              Type: published
              Y: 2026
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            – TitleFull: Materials (1996-1944)
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