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Determination of acrylamide in food by solid-phase microextraction coupled to gas chromatography–positive chemical ionization tandem mass spectrometry

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Title: Determination of acrylamide in food by solid-phase microextraction coupled to gas chromatography–positive chemical ionization tandem mass spectrometry
Authors: Lee, Maw-Rong1 mrlee@dragon.nchu.edu.tw, Chang, Li-Yo1, Dou, Jianpeng1,2
Source: Analytica Chimica Acta. Jan2007, Vol. 582 Issue 1, p19-23. 5p.
Subjects: Chromatographic analysis, Acrylamide, Gas chromatography, Scission (Chemistry)
Abstract: Abstract: A method has been developed to determine acrylamide in aqueous matrices by using direct immersion solid-phase microextraction (SPME) coupled to gas chromatography–positive chemical ionization tandem mass spectrometry (GC–PCI-MS–MS) in the selected reaction monitoring (SRM) mode. The optimized SPME experimental procedures to extract acrylamide in water solutions were: use of a carbowax/divinylbenzene (CW/DVB)-coated fiber at pH 7, extraction time of 20min and analyte desorption at 210°C for 3min. A detection limit of 0.1μgL−1 was obtained. The linear range was 1–1000μgL−1. The relative standard deviation was 10.64% (n =7). The proposed analytical method was successfully used for the quantification of trace acrylamide in foodstuffs such as French fries (1.2μgg−1) and potato crisps (2.2μgg−1). [Copyright &y& Elsevier]
Copyright of Analytica Chimica Acta is the property of Elsevier B.V. and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)
Database: Engineering Source
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DbLabel: Engineering Source
An: 23448572
AccessLevel: 6
PubType: Academic Journal
PubTypeId: academicJournal
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  Data: Determination of acrylamide in food by solid-phase microextraction coupled to gas chromatography–positive chemical ionization tandem mass spectrometry
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  Data: <searchLink fieldCode="AR" term="%22Lee%2C+Maw-Rong%22">Lee, Maw-Rong</searchLink><relatesTo>1</relatesTo><i> mrlee@dragon.nchu.edu.tw</i><br /><searchLink fieldCode="AR" term="%22Chang%2C+Li-Yo%22">Chang, Li-Yo</searchLink><relatesTo>1</relatesTo><br /><searchLink fieldCode="AR" term="%22Dou%2C+Jianpeng%22">Dou, Jianpeng</searchLink><relatesTo>1,2</relatesTo>
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  Data: <searchLink fieldCode="JN" term="%22Analytica+Chimica+Acta%22">Analytica Chimica Acta</searchLink>. Jan2007, Vol. 582 Issue 1, p19-23. 5p.
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  Data: <searchLink fieldCode="DE" term="%22Chromatographic+analysis%22">Chromatographic analysis</searchLink><br /><searchLink fieldCode="DE" term="%22Acrylamide%22">Acrylamide</searchLink><br /><searchLink fieldCode="DE" term="%22Gas+chromatography%22">Gas chromatography</searchLink><br /><searchLink fieldCode="DE" term="%22Scission+%28Chemistry%29%22">Scission (Chemistry)</searchLink>
– Name: Abstract
  Label: Abstract
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  Data: Abstract: A method has been developed to determine acrylamide in aqueous matrices by using direct immersion solid-phase microextraction (SPME) coupled to gas chromatography–positive chemical ionization tandem mass spectrometry (GC–PCI-MS–MS) in the selected reaction monitoring (SRM) mode. The optimized SPME experimental procedures to extract acrylamide in water solutions were: use of a carbowax/divinylbenzene (CW/DVB)-coated fiber at pH 7, extraction time of 20min and analyte desorption at 210°C for 3min. A detection limit of 0.1μgL−1 was obtained. The linear range was 1–1000μgL−1. The relative standard deviation was 10.64% (n =7). The proposed analytical method was successfully used for the quantification of trace acrylamide in foodstuffs such as French fries (1.2μgg−1) and potato crisps (2.2μgg−1). [Copyright &y& Elsevier]
– Name: AbstractSuppliedCopyright
  Label:
  Group: Ab
  Data: <i>Copyright of Analytica Chimica Acta is the property of Elsevier B.V. and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.)
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        Value: 10.1016/j.aca.2006.08.042
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        Text: English
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        Type: general
      – SubjectFull: Acrylamide
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      – SubjectFull: Gas chromatography
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              Text: Jan2007
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