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A new synthetic route towards a Ru(III) substituted heteropolytungstate anion

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Title: A new synthetic route towards a Ru(III) substituted heteropolytungstate anion
Authors: Besson, Claire1, Chen, Su-Wen1, Villanneau, Richard1, Izzet, Guillaume guillaume.izzet@upmc.fr, Proust, Anna
Source: Inorganic Chemistry Communications. Oct2009, Vol. 12 Issue 10, p1042-1044. 3p.
Subjects: Ruthenium compounds, Polytungstates, Complex compounds synthesis, Microwaves, Irradiation, Ammonium salts, X-ray absorption near edge structure, Electron paramagnetic resonance spectroscopy
Abstract: Abstract: Microwave irradiation of a mixture of K7[PW11O39]·14H2O and [Ru(dmf)6](CF3SO3)3 allowed the straightforward hydrothermal synthesis of the Keggin-type [PW11O39RuIII(OH2)]4− anion. Physical characterizations of the corresponding tetrabutylammonium (TBA) salt are herein described. This study provides a complete set of spectroscopic and electrochemical references for RuIII-incorporating heteropolytungstates. [Copyright &y& Elsevier]
Copyright of Inorganic Chemistry Communications is the property of Elsevier B.V. and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)
Database: Engineering Source
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DbLabel: Engineering Source
An: 44473328
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PubTypeId: academicJournal
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  Data: <searchLink fieldCode="JN" term="%22Inorganic+Chemistry+Communications%22">Inorganic Chemistry Communications</searchLink>. Oct2009, Vol. 12 Issue 10, p1042-1044. 3p.
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  Data: <searchLink fieldCode="DE" term="%22Ruthenium+compounds%22">Ruthenium compounds</searchLink><br /><searchLink fieldCode="DE" term="%22Polytungstates%22">Polytungstates</searchLink><br /><searchLink fieldCode="DE" term="%22Complex+compounds+synthesis%22">Complex compounds synthesis</searchLink><br /><searchLink fieldCode="DE" term="%22Microwaves%22">Microwaves</searchLink><br /><searchLink fieldCode="DE" term="%22Irradiation%22">Irradiation</searchLink><br /><searchLink fieldCode="DE" term="%22Ammonium+salts%22">Ammonium salts</searchLink><br /><searchLink fieldCode="DE" term="%22X-ray+absorption+near+edge+structure%22">X-ray absorption near edge structure</searchLink><br /><searchLink fieldCode="DE" term="%22Electron+paramagnetic+resonance+spectroscopy%22">Electron paramagnetic resonance spectroscopy</searchLink>
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  Data: Abstract: Microwave irradiation of a mixture of K7[PW11O39]·14H2O and [Ru(dmf)6](CF3SO3)3 allowed the straightforward hydrothermal synthesis of the Keggin-type [PW11O39RuIII(OH2)]4− anion. Physical characterizations of the corresponding tetrabutylammonium (TBA) salt are herein described. This study provides a complete set of spectroscopic and electrochemical references for RuIII-incorporating heteropolytungstates. [Copyright &y& Elsevier]
– Name: AbstractSuppliedCopyright
  Label:
  Group: Ab
  Data: <i>Copyright of Inorganic Chemistry Communications is the property of Elsevier B.V. and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.</i> (Copyright applies to all Abstracts.)
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      – Type: doi
        Value: 10.1016/j.inoche.2009.08.016
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      – Code: eng
        Text: English
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        PageCount: 3
        StartPage: 1042
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      – SubjectFull: Ruthenium compounds
        Type: general
      – SubjectFull: Polytungstates
        Type: general
      – SubjectFull: Complex compounds synthesis
        Type: general
      – SubjectFull: Microwaves
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      – SubjectFull: Irradiation
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      – SubjectFull: Ammonium salts
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      – SubjectFull: X-ray absorption near edge structure
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      – SubjectFull: Electron paramagnetic resonance spectroscopy
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      – TitleFull: A new synthetic route towards a Ru(III) substituted heteropolytungstate anion
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              M: 10
              Text: Oct2009
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