Adamantyl-group containing mixed-mode acrylamide-based continuous beds for capillary electrochromatography. Part II. Characterization of the synthesized monoliths by inverse size exclusion chromatography and scanning electron microscopy.

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Title: Adamantyl-group containing mixed-mode acrylamide-based continuous beds for capillary electrochromatography. Part II. Characterization of the synthesized monoliths by inverse size exclusion chromatography and scanning electron microscopy.
Authors: “Ayat Allah” Al-Massaedh1, Pyell, Ute1 pyellu@staff.uni-marburg.de
Source: Journal of Chromatography A. Jan2014, Vol. 1325, p247-255. 9p.
Subjects: Adamantane, Capillary electrochromatography, Acrylamide synthesis, Gel permeation chromatography, Scanning electron microscopy, Pore size distribution
Abstract: Highlights: [•] Characterization of the domain size of acrylamide-based continuous beds by SEM. [•] Measurement of pore size distributions and exclusion pore sizes by ISEC. [•] The impact of the concentration of AS on morphology, pore size distribution, and pore volumes is studied. [•] For monoliths with small domain size a trimodal pore size distribution is confirmed. [•] An excellent capillary-to-capillary, day-to-day, and run-to-run repeatability is reached. [ABSTRACT FROM AUTHOR]
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Database: Engineering Source
Description
Abstract:Highlights: [•] Characterization of the domain size of acrylamide-based continuous beds by SEM. [•] Measurement of pore size distributions and exclusion pore sizes by ISEC. [•] The impact of the concentration of AS on morphology, pore size distribution, and pore volumes is studied. [•] For monoliths with small domain size a trimodal pore size distribution is confirmed. [•] An excellent capillary-to-capillary, day-to-day, and run-to-run repeatability is reached. [ABSTRACT FROM AUTHOR]
ISSN:00219673
DOI:10.1016/j.chroma.2013.12.026