Physicochemical properties of calcium silicate-based endodontic sealers: comparative analysis of distinct compositions.

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Title: Physicochemical properties of calcium silicate-based endodontic sealers: comparative analysis of distinct compositions.
Alternate Title: Propriedades físico-químicas de cimentos endodônticos à base de silicato de cálcio: análise comparativa de composições distintas.
Authors: Cristina VERTUAN, Gislene1, de OLIVEIRA NETO, Raimundo Sales1 cdraimundoneto@hotmail.com, Ferreira da SILVA, Guilherme1, Ricci VIVAN, Rodrigo1, Priori ALCALDE, Murilo1, Hungaro DUARTE, Marco Antonio1
Source: Dental Press Endodontics. Jan-Apr2025, Vol. 15 Issue 1, p108-129. 44p.
Subjects: PIT & fissure sealants (Dentistry), ROOT canal treatment, MATERIALS testing, RADIOPACITY, DISTILLED water
Abstract (English): OBJECTIVE: This study aimed to evaluate the physicochemical properties of calcium silicate-based root canal sealers (powder/liquid), including three experimental sealers (CE1, CE2, CE3), BioRoot RCS (BR), CIMMO HP® (CHP), Sealer Plus BC (SPBC), and BioLine Sealer Z (BLZ). METHODS: Setting time (ASTM C266/2008), Radiopacity (ANSI/ADA #57 and ISO 6876 standards), flow, and pH (1.0×10.0 mm tubes immersed in distilled water for 3, 24, 72, and 168 h) were analyzed, with a significance level of 5%. RESULTS: CE1 and CE2 exhibited higher radiopacity (p<0.05), with no significant difference between them (p>0.05). In contrast, CHP and BLZ had the lowest values (p<0.05). CE1 and CE3 exhibited greater flow (p<0.05). The experimental sealers (CE1, CH2, and CE3) demonstrated the shortest initial and final setting times (p<0.05), in contrast to SPBC and BLZ, which showed the longest (p<0.05). All materials alkalized the medium after 168 h, except CE1. CONCLUSIONS: The BLZ sealer did not meet the minimum radiopacity requirements of ISO standards, requiring reformulation. The experimental sealers stood out for their reduced setting times and greater flow. All sealers promoted medium alkalization, except CE1. [ABSTRACT FROM AUTHOR]
Abstract (Portuguese): OBJETIVO: O objetivo desse estudo foi avaliar as propriedades físico- químicas de cimentos obturadores à base de silicato de cálcio (pó/líquido), incluindo três cimentos experimentais (CE1, CE2, CE3), BioRoot RCS (BR), CIMMO HP® (CHP), Sealer Plus BC (SPBC) e BioLine Sealer Z (BLZ). MÉTODOS: Foram analisados tempo de presa (ASTM C266/2008), radiopacidade (normas ANSI/ADA nº57 e ISO 6876), escoamento, e pH (tubos de 1,0 × 10,0 mm imersos em água destilada, avaliados nos períodos experimentais de 3, 24, 72 e 168 h). O nível de significância estatística foi estabelecido em 5%. RESULTADOS: CE1 e CE2 apresentaram maior radiopacidade (p<0,05), sem diferença entre si (p>0,05), enquanto CHP e BLZ tiveram os menores valores (p<0,05). CE1 e CE3 exibiram maior escoamento (p<0,05). Os cimentos experimentais (CE1, CE2 e CE3) demonstraram os menores tempos de presa inicial e final (p<0,05), contrastando com SPBC e BLZ, que apresentaram os maiores (p<0,05). Todos os materiais alcalinizaram o meio após 168 h, exceto o CE1. CONCLUSÕES: O cimento BLZ não atendeu aos requisitos mínimos de radiopacidade das normas ISO, necessitando reformulação. Os cimentos experimentais destacaram-se por tempos de presa reduzidos e maior escoamento. Todos os cimentos promoveram a alcalinização do meio, exceto o CE1. [ABSTRACT FROM AUTHOR]
Copyright of Dental Press Endodontics is the property of Dental Press International and its content may not be copied or emailed to multiple sites without the copyright holder's express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract. (Copyright applies to all Abstracts.)
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  Data: Physicochemical properties of calcium silicate-based endodontic sealers: comparative analysis of distinct compositions.
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  Data: Propriedades f&#237;sico-qu&#237;micas de cimentos endod&#244;nticos &#224; base de silicato de c&#225;lcio: an&#225;lise comparativa de composi&#231;&#245;es distintas.
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  Data: &lt;searchLink fieldCode=&quot;AR&quot; term=&quot;%22Cristina+VERTUAN%2C+Gislene%22&quot;&gt;Cristina VERTUAN, Gislene&lt;/searchLink&gt;&lt;relatesTo&gt;1&lt;/relatesTo&gt;&lt;br /&gt;&lt;searchLink fieldCode=&quot;AR&quot; term=&quot;%22de+OLIVEIRA+NETO%2C+Raimundo+Sales%22&quot;&gt;de OLIVEIRA NETO, Raimundo Sales&lt;/searchLink&gt;&lt;relatesTo&gt;1&lt;/relatesTo&gt;&lt;i&gt; cdraimundoneto@hotmail.com&lt;/i&gt;&lt;br /&gt;&lt;searchLink fieldCode=&quot;AR&quot; term=&quot;%22Ferreira+da+SILVA%2C+Guilherme%22&quot;&gt;Ferreira da SILVA, Guilherme&lt;/searchLink&gt;&lt;relatesTo&gt;1&lt;/relatesTo&gt;&lt;br /&gt;&lt;searchLink fieldCode=&quot;AR&quot; term=&quot;%22Ricci+VIVAN%2C+Rodrigo%22&quot;&gt;Ricci VIVAN, Rodrigo&lt;/searchLink&gt;&lt;relatesTo&gt;1&lt;/relatesTo&gt;&lt;br /&gt;&lt;searchLink fieldCode=&quot;AR&quot; term=&quot;%22Priori+ALCALDE%2C+Murilo%22&quot;&gt;Priori ALCALDE, Murilo&lt;/searchLink&gt;&lt;relatesTo&gt;1&lt;/relatesTo&gt;&lt;br /&gt;&lt;searchLink fieldCode=&quot;AR&quot; term=&quot;%22Hungaro+DUARTE%2C+Marco+Antonio%22&quot;&gt;Hungaro DUARTE, Marco Antonio&lt;/searchLink&gt;&lt;relatesTo&gt;1&lt;/relatesTo&gt;
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  Data: &lt;searchLink fieldCode=&quot;JN&quot; term=&quot;%22Dental+Press+Endodontics%22&quot;&gt;Dental Press Endodontics&lt;/searchLink&gt;. Jan-Apr2025, Vol. 15 Issue 1, p108-129. 44p.
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  Data: &lt;searchLink fieldCode=&quot;DE&quot; term=&quot;%22PIT+%26+fissure+sealants+%28Dentistry%29%22&quot;&gt;PIT &amp; fissure sealants (Dentistry)&lt;/searchLink&gt;&lt;br /&gt;&lt;searchLink fieldCode=&quot;DE&quot; term=&quot;%22ROOT+canal+treatment%22&quot;&gt;ROOT canal treatment&lt;/searchLink&gt;&lt;br /&gt;&lt;searchLink fieldCode=&quot;DE&quot; term=&quot;%22MATERIALS+testing%22&quot;&gt;MATERIALS testing&lt;/searchLink&gt;&lt;br /&gt;&lt;searchLink fieldCode=&quot;DE&quot; term=&quot;%22RADIOPACITY%22&quot;&gt;RADIOPACITY&lt;/searchLink&gt;&lt;br /&gt;&lt;searchLink fieldCode=&quot;DE&quot; term=&quot;%22DISTILLED+water%22&quot;&gt;DISTILLED water&lt;/searchLink&gt;
– Name: Abstract
  Label: Abstract (English)
  Group: Ab
  Data: OBJECTIVE: This study aimed to evaluate the physicochemical properties of calcium silicate-based root canal sealers (powder/liquid), including three experimental sealers (CE1, CE2, CE3), BioRoot RCS (BR), CIMMO HP&#174; (CHP), Sealer Plus BC (SPBC), and BioLine Sealer Z (BLZ). METHODS: Setting time (ASTM C266/2008), Radiopacity (ANSI/ADA #57 and ISO 6876 standards), flow, and pH (1.0&#215;10.0 mm tubes immersed in distilled water for 3, 24, 72, and 168 h) were analyzed, with a significance level of 5%. RESULTS: CE1 and CE2 exhibited higher radiopacity (p&lt;0.05), with no significant difference between them (p&gt;0.05). In contrast, CHP and BLZ had the lowest values (p&lt;0.05). CE1 and CE3 exhibited greater flow (p&lt;0.05). The experimental sealers (CE1, CH2, and CE3) demonstrated the shortest initial and final setting times (p&lt;0.05), in contrast to SPBC and BLZ, which showed the longest (p&lt;0.05). All materials alkalized the medium after 168 h, except CE1. CONCLUSIONS: The BLZ sealer did not meet the minimum radiopacity requirements of ISO standards, requiring reformulation. The experimental sealers stood out for their reduced setting times and greater flow. All sealers promoted medium alkalization, except CE1. [ABSTRACT FROM AUTHOR]
– Name: Abstract
  Label: Abstract (Portuguese)
  Group: Ab
  Data: OBJETIVO: O objetivo desse estudo foi avaliar as propriedades f&#237;sico- qu&#237;micas de cimentos obturadores &#224; base de silicato de c&#225;lcio (p&#243;/l&#237;quido), incluindo tr&#234;s cimentos experimentais (CE1, CE2, CE3), BioRoot RCS (BR), CIMMO HP&#174; (CHP), Sealer Plus BC (SPBC) e BioLine Sealer Z (BLZ). M&#201;TODOS: Foram analisados tempo de presa (ASTM C266/2008), radiopacidade (normas ANSI/ADA n&#186;57 e ISO 6876), escoamento, e pH (tubos de 1,0 &#215; 10,0 mm imersos em &#225;gua destilada, avaliados nos per&#237;odos experimentais de 3, 24, 72 e 168 h). O n&#237;vel de signific&#226;ncia estat&#237;stica foi estabelecido em 5%. RESULTADOS: CE1 e CE2 apresentaram maior radiopacidade (p&lt;0,05), sem diferen&#231;a entre si (p&gt;0,05), enquanto CHP e BLZ tiveram os menores valores (p&lt;0,05). CE1 e CE3 exibiram maior escoamento (p&lt;0,05). Os cimentos experimentais (CE1, CE2 e CE3) demonstraram os menores tempos de presa inicial e final (p&lt;0,05), contrastando com SPBC e BLZ, que apresentaram os maiores (p&lt;0,05). Todos os materiais alcalinizaram o meio ap&#243;s 168 h, exceto o CE1. CONCLUS&#213;ES: O cimento BLZ n&#227;o atendeu aos requisitos m&#237;nimos de radiopacidade das normas ISO, necessitando reformula&#231;&#227;o. Os cimentos experimentais destacaram-se por tempos de presa reduzidos e maior escoamento. Todos os cimentos promoveram a alcaliniza&#231;&#227;o do meio, exceto o CE1. [ABSTRACT FROM AUTHOR]
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  Data: &lt;i&gt;Copyright of Dental Press Endodontics is the property of Dental Press International and its content may not be copied or emailed to multiple sites without the copyright holder&#39;s express written permission. Additionally, content may not be used with any artificial intelligence tools or machine learning technologies. However, users may print, download, or email articles for individual use. This abstract may be abridged. No warranty is given about the accuracy of the copy. Users should refer to the original published version of the material for the full abstract.&lt;/i&gt; (Copyright applies to all Abstracts.)
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        Value: 10.14436/2358-2545.15.1.108-129.oar
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      – Code: eng
        Text: English
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    Subjects:
      – SubjectFull: PIT & fissure sealants (Dentistry)
        Type: general
      – SubjectFull: ROOT canal treatment
        Type: general
      – SubjectFull: MATERIALS testing
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      – SubjectFull: RADIOPACITY
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      – SubjectFull: DISTILLED water
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      – TitleFull: Physicochemical properties of calcium silicate-based endodontic sealers: comparative analysis of distinct compositions.
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            NameFull: Cristina VERTUAN, Gislene
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              M: 01
              Text: Jan-Apr2025
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              Y: 2025
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