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Fabrication and characterization of ceramic coatings with alumina–silica sol-incorporated α-alumina powder coated on woven quartz fiber fabrics.

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Title: Fabrication and characterization of ceramic coatings with alumina–silica sol-incorporated α-alumina powder coated on woven quartz fiber fabrics.
Authors: Lu, Hao-Ran1, Wang, Chang-An1 wangca888@126.com
Source: Ceramics International. Aug2013, Vol. 39 Issue 6, p6041-6050. 10p.
Subjects: Microfabrication, Ceramic metals, Metal coating, Aluminum oxide, Silica, Sol-gel processes, Metal powders, Quartz fibers, Particle size distribution, X-ray diffraction
Abstract: Abstract: The formation and properties of dense silica/α-alumina coatings derived from alumina–silica sol-incorporated coarse alumina powder (median particle size d 50=0.509μm) using Al(NO3)3·9H2O and tetraethyl orthosilicate as precursors have been investigated. Phase compositions and thermal evolution analysis of the coatings as well as interface microstructure between the coatings and the matrix were characterized by means of XRD, XRF, DSC-TG, TEM, SEM supplemented with EDS, and tensile strength tester. Silica/α-alumina coatings combined with quartz fiber matrix are homogeneously integrated with distinct inter-diffusion near the interface. The heat conduction mechanism of the quartz fiber matrix was influenced by the dense silica/α-alumina ceramic coatings, and the prepared coatings provide practical thermodynamic stability and desired mechanical strength for the woven quartz fiber fabrics. [Copyright &y& Elsevier]
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Database: Engineering Source
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Abstract:Abstract: The formation and properties of dense silica/α-alumina coatings derived from alumina–silica sol-incorporated coarse alumina powder (median particle size d 50=0.509μm) using Al(NO3)3·9H2O and tetraethyl orthosilicate as precursors have been investigated. Phase compositions and thermal evolution analysis of the coatings as well as interface microstructure between the coatings and the matrix were characterized by means of XRD, XRF, DSC-TG, TEM, SEM supplemented with EDS, and tensile strength tester. Silica/α-alumina coatings combined with quartz fiber matrix are homogeneously integrated with distinct inter-diffusion near the interface. The heat conduction mechanism of the quartz fiber matrix was influenced by the dense silica/α-alumina ceramic coatings, and the prepared coatings provide practical thermodynamic stability and desired mechanical strength for the woven quartz fiber fabrics. [Copyright &y& Elsevier]
ISSN:02728842
DOI:10.1016/j.ceramint.2013.01.020