Confocal two photon emission microscopy: A new approach to waveguide imaging

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Bibliographic Details
Title: Confocal two photon emission microscopy: A new approach to waveguide imaging
Authors: Dierolf, V. vod2@lehigh.edu, Sandmann, C.1
Source: Journal of Luminescence. May2003, Vol. 102-103, p201. 5p.
Subjects: Confocal microscopy, Integrated optics, Waveguides
Abstract: Based on earlier studies of the interaction effects between Er3+ and Ti4+ ions in Ti:LiNbO3 waveguides we investigated the feasibility of using the Er3+ as a sensitive probe to determine Ti4+-diffusion profiles with high spatial resolution. Using a home-built confocal microscope combined with site-selective optical spectroscopy we tested two different operation modes: (i) Evaluating the emission spectra obtained by one-step excitation with a single laser we obtain high resolution (≈700 nm) Ti4+-concentration images. In particular using the second moments of the spectra, which turn out to be approximately linearly related to the Ti4+-concentration, we obtain very good contrast with essentially no artifacts caused by topology, intensity fluctuations, and Er3+ ion concentration profile. (ii) Measuring the total emission intensity under a specially chosen two step excitation scheme allows to selectively excite regions with a certain Ti4+ concentration. While for (i) a calibration can be done, for (ii) this will be hard due to the multi-site character of the Er3+ in LiNbO3. [Copyright &y& Elsevier]
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Database: Engineering Source
Description
Abstract:Based on earlier studies of the interaction effects between <f>Er3+</f> and <f>Ti4+</f> ions in <f>Ti:LiNbO3</f> waveguides we investigated the feasibility of using the <f>Er3+</f> as a sensitive probe to determine <f>Ti4+</f>-diffusion profiles with high spatial resolution. Using a home-built confocal microscope combined with site-selective optical spectroscopy we tested two different operation modes: (i) Evaluating the emission spectra obtained by one-step excitation with a single laser we obtain high resolution <f>(&ap;700 nm) Ti4+</f>-concentration images. In particular using the second moments of the spectra, which turn out to be approximately linearly related to the <f>Ti4+</f>-concentration, we obtain very good contrast with essentially no artifacts caused by topology, intensity fluctuations, and <f>Er3+</f> ion concentration profile. (ii) Measuring the total emission intensity under a specially chosen two step excitation scheme allows to selectively excite regions with a certain <f>Ti4+</f> concentration. While for (i) a calibration can be done, for (ii) this will be hard due to the multi-site character of the <f>Er3+</f> in <f>LiNbO3</f>. [Copyright &y& Elsevier]
ISSN:00222313
DOI:10.1016/S0022-2313(02)00491-X