Fast determination of 22 sulfonamides from chicken breast muscle using core–shell nanoring amino-functionalized superparamagnetic molecularly imprinted polymer followed by liquid chromatography-tandem mass spectrometry.

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Title: Fast determination of 22 sulfonamides from chicken breast muscle using core–shell nanoring amino-functionalized superparamagnetic molecularly imprinted polymer followed by liquid chromatography-tandem mass spectrometry.
Authors: Zhao, Yong-Gang1,2, Zhou, Li-Xin3, Pan, Sheng-Dong1,2, Zhan, Ping-Ping4, Chen, Xiao-Hong1,2, Jin, Mi-Cong1,2 jmcjc@163.com
Source: Journal of Chromatography A. Jun2014, Vol. 1345, p17-28. 12p.
Subjects: Sulfonamides, Chickens, Nanostructured materials, Amino compounds, Superparamagnetic materials, Molecular imprinting, Imprinted polymers, Liquid chromatography-mass spectrometry, Physiology
Abstract: Highlights: [•] An effective d-μ-SPE procedure with CS-NR-Mag-MIP adsorbent has been developed for extraction of 22 SAs. [•] The proposed sample preparation procedure is environmental friendly, less time and solvent-consuming. [•] A novel d-μ-SPE UFLC-MS/MS method for analysis of 22 SAs in chicken breast muscle has been developed. [•] LOQs are significantly lower than other reported LC-MS/MS-based methodologies. [ABSTRACT FROM AUTHOR]
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Database: Engineering Source
Description
Abstract:Highlights: [•] An effective d-μ-SPE procedure with CS-NR-Mag-MIP adsorbent has been developed for extraction of 22 SAs. [•] The proposed sample preparation procedure is environmental friendly, less time and solvent-consuming. [•] A novel d-μ-SPE UFLC-MS/MS method for analysis of 22 SAs in chicken breast muscle has been developed. [•] LOQs are significantly lower than other reported LC-MS/MS-based methodologies. [ABSTRACT FROM AUTHOR]
ISSN:00219673
DOI:10.1016/j.chroma.2014.04.028