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Simple and Inexpensive Method for the Detection of Carbon Monoxide Released from Thermal Cheletropic Decarbonylation Reactions

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Bibliographic Details
Title: Simple and Inexpensive Method for the Detection of Carbon Monoxide Released from Thermal Cheletropic Decarbonylation Reactions
Language: English
Authors: Smellie, Iain A. (ORCID 0000-0002-5829-6487), Carpenter-Warren, Cameron L., Chalmers, Brian A. (ORCID 0000-0002-2999-2272), Cordes, David B. (ORCID 0000-0002-5366-9168), F. De A. Gouy, Rodrigo P., Keddie, Neil S. (ORCID 0000-0002-9502-5862), Lebl, Tomas (ORCID 0000-0002-0269-3221), Patterson, Iain. L. J., Slawin, Alexandra M. Z.
Source: Journal of Chemical Education. Nov 2021 98(11):3608-3613.
Availability: Division of Chemical Education, Inc. and ACS Publications Division of the American Chemical Society. 1155 Sixteenth Street NW, Washington, DC 20036. Tel: 800-227-5558; Tel: 202-872-4600; e-mail: eic@jce.acs.org; Web site: http://pubs.acs.org/jchemeduc
Peer Reviewed: Y
Page Count: 6
Publication Date: 2021
Document Type: Journal Articles
Reports - Descriptive
Education Level: Higher Education
Postsecondary Education
Descriptors: Science Instruction, Scientific Concepts, Concept Formation, Chemistry, Science Laboratories, College Science, Teaching Methods, Measurement Equipment, Hazardous Materials
DOI: 10.1021/acs.jchemed.1c00517
ISSN: 0021-9584
Abstract: This work presents a simple protocol that demonstrates the use of an inexpensive household carbon monoxide detector as a useful tool to detect the release of carbon monoxide gas from thermal cheletropic decarbonylation reactions. The carbon monoxide detection method described has been employed in a short series of reactions used in a university teaching laboratory setting, and full procedures for these are outlined. In each case, the procedure to isolate and identify the decarbonylation products has also been provided.
Abstractor: As Provided
Entry Date: 2021
Accession Number: EJ1316460
Database: ERIC
Description
Abstract:This work presents a simple protocol that demonstrates the use of an inexpensive household carbon monoxide detector as a useful tool to detect the release of carbon monoxide gas from thermal cheletropic decarbonylation reactions. The carbon monoxide detection method described has been employed in a short series of reactions used in a university teaching laboratory setting, and full procedures for these are outlined. In each case, the procedure to isolate and identify the decarbonylation products has also been provided.
ISSN:0021-9584
DOI:10.1021/acs.jchemed.1c00517