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Simple and Inexpensive Method for the Detection of Carbon Monoxide Released from Thermal Cheletropic Decarbonylation Reactions

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Title: Simple and Inexpensive Method for the Detection of Carbon Monoxide Released from Thermal Cheletropic Decarbonylation Reactions
Language: English
Authors: Smellie, Iain A. (ORCID 0000-0002-5829-6487), Carpenter-Warren, Cameron L., Chalmers, Brian A. (ORCID 0000-0002-2999-2272), Cordes, David B. (ORCID 0000-0002-5366-9168), F. De A. Gouy, Rodrigo P., Keddie, Neil S. (ORCID 0000-0002-9502-5862), Lebl, Tomas (ORCID 0000-0002-0269-3221), Patterson, Iain. L. J., Slawin, Alexandra M. Z.
Source: Journal of Chemical Education. Nov 2021 98(11):3608-3613.
Availability: Division of Chemical Education, Inc. and ACS Publications Division of the American Chemical Society. 1155 Sixteenth Street NW, Washington, DC 20036. Tel: 800-227-5558; Tel: 202-872-4600; e-mail: eic@jce.acs.org; Web site: http://pubs.acs.org/jchemeduc
Peer Reviewed: Y
Page Count: 6
Publication Date: 2021
Document Type: Journal Articles
Reports - Descriptive
Education Level: Higher Education
Postsecondary Education
Descriptors: Science Instruction, Scientific Concepts, Concept Formation, Chemistry, Science Laboratories, College Science, Teaching Methods, Measurement Equipment, Hazardous Materials
DOI: 10.1021/acs.jchemed.1c00517
ISSN: 0021-9584
Abstract: This work presents a simple protocol that demonstrates the use of an inexpensive household carbon monoxide detector as a useful tool to detect the release of carbon monoxide gas from thermal cheletropic decarbonylation reactions. The carbon monoxide detection method described has been employed in a short series of reactions used in a university teaching laboratory setting, and full procedures for these are outlined. In each case, the procedure to isolate and identify the decarbonylation products has also been provided.
Abstractor: As Provided
Entry Date: 2021
Accession Number: EJ1316460
Database: ERIC
FullText Text:
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  Data: Simple and Inexpensive Method for the Detection of Carbon Monoxide Released from Thermal Cheletropic Decarbonylation Reactions
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  Data: <searchLink fieldCode="AR" term="%22Smellie%2C+Iain+A%2E%22">Smellie, Iain A.</searchLink> (ORCID <externalLink term="https://orcid.org/0000-0002-5829-6487">0000-0002-5829-6487</externalLink>)<br /><searchLink fieldCode="AR" term="%22Carpenter-Warren%2C+Cameron+L%2E%22">Carpenter-Warren, Cameron L.</searchLink><br /><searchLink fieldCode="AR" term="%22Chalmers%2C+Brian+A%2E%22">Chalmers, Brian A.</searchLink> (ORCID <externalLink term="https://orcid.org/0000-0002-2999-2272">0000-0002-2999-2272</externalLink>)<br /><searchLink fieldCode="AR" term="%22Cordes%2C+David+B%2E%22">Cordes, David B.</searchLink> (ORCID <externalLink term="https://orcid.org/0000-0002-5366-9168">0000-0002-5366-9168</externalLink>)<br /><searchLink fieldCode="AR" term="%22F%2E+De+A%2E+Gouy%2C+Rodrigo+P%2E%22">F. De A. Gouy, Rodrigo P.</searchLink><br /><searchLink fieldCode="AR" term="%22Keddie%2C+Neil+S%2E%22">Keddie, Neil S.</searchLink> (ORCID <externalLink term="https://orcid.org/0000-0002-9502-5862">0000-0002-9502-5862</externalLink>)<br /><searchLink fieldCode="AR" term="%22Lebl%2C+Tomas%22">Lebl, Tomas</searchLink> (ORCID <externalLink term="https://orcid.org/0000-0002-0269-3221">0000-0002-0269-3221</externalLink>)<br /><searchLink fieldCode="AR" term="%22Patterson%2C+Iain%2E+L%2E+J%2E%22">Patterson, Iain. L. J.</searchLink><br /><searchLink fieldCode="AR" term="%22Slawin%2C+Alexandra+M%2E+Z%2E%22">Slawin, Alexandra M. Z.</searchLink>
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  Data: Division of Chemical Education, Inc. and ACS Publications Division of the American Chemical Society. 1155 Sixteenth Street NW, Washington, DC 20036. Tel: 800-227-5558; Tel: 202-872-4600; e-mail: eic@jce.acs.org; Web site: http://pubs.acs.org/jchemeduc
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  Data: 10.1021/acs.jchemed.1c00517
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  Data: This work presents a simple protocol that demonstrates the use of an inexpensive household carbon monoxide detector as a useful tool to detect the release of carbon monoxide gas from thermal cheletropic decarbonylation reactions. The carbon monoxide detection method described has been employed in a short series of reactions used in a university teaching laboratory setting, and full procedures for these are outlined. In each case, the procedure to isolate and identify the decarbonylation products has also been provided.
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  Data: 2021
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  Data: EJ1316460
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